908093-98-1合成路线 （共 442 条）
反应条件
in tetrahydrofuran soln. of Ti complex in THF reacted with neat Ph2CN2 under N2, heated until all ppt. dissolved; (CpTiCl)2(NNCPh2)2 crystd. from resulting soln., filtered soln. evapd., residue collected with toluene and heated, suspn. filtered when hot, added hexane, CpTiCl3 crystd. from this soln.;
参考文献
Journal of the American Chemical Society, , vol. 105, # 25 p. 7295 - 7301
反应条件
oxygen in acetonitrile T=25°C; Product distribution;
参考文献
Russian Chemical Bulletin, , vol. 49, # 9 p. 1496 - 1500
反应条件
P-Rose Bengal; oxygen in dichloromethane T=5°C; Irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Kumar, Shailendra; Murray, Robert W.
Tetrahedron Letters, 1980 , vol. 21, p. 4781 - 4782
参考文献
Burgess, Laurence E.; Koch, Kevin; Cooper, Kelvin; Biggers, Michael S.; Ramchandani, Mukesh; Smitrovich, Jacqueline H.; Gilbert, Eric J.; Bruns, Matthew J.; Mather, Robert J.; Donovan, Carol B.; Hanson, Douglas C.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 8 p. 1047 - 1052
反应条件
1: With copper(l) iodide; cesium fluoride in 1,4-dioxane; 1-methyl-pyrrolidin-2-one T=20°C; 0.5 h; GloveboxSchlenk technique; 2: in 1,4-dioxane; 1-methyl-pyrrolidin-2-one T=20°C; 20 h; GloveboxSchlenk technique; Solvent;
参考文献
Hu, Mingyou; He, Zhengbiao; Gao, Bing; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17302 - 17305
参考文献
Middleton,W.J. et al.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 1193 - 1197
参考文献
Merck and Co.Inc.
Patent: US2595405 , 1949 ;
反应条件
TPP; oxygen in benzene 0.166667 h; Ambient temperatureIrradiation;
参考文献
Journal of Organic Chemistry, , vol. 47, # 15 p. 2900 - 2903
反应条件
Petroleum ether im geschlossenen Rohr;
参考文献
Staudinger; Anthes; Pfenninger
Chemische Berichte, 1916 , vol. 49, p. 1939
反应条件
copper acetylacetonate in benzene 1 h; Heating;
参考文献
Polozov; Polezhaeva; Mustaphin; Khotinen; Arbuzov
Synthesis, 1990 , # 6 p. 515 - 517
