908093-98-1合成路线 (共 442 条)
反应条件
in tetrachloromethane
3 h; Heating;
参考文献
Doyle, Michael P.; Devia, Alvaro H.; Bassett, Kathlene E.; Terpstra, Jan W.; Mahapatro, Surendra N.
Journal of Organic Chemistry, 1987 , vol. 52, # 8 p. 1619 - 1621
反应条件
in dichloromethane
T=20°C; 72 h;
参考文献
Grant, Jonathan W.; Smyth, Timothy P.
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 7965 - 7970
反应条件
in 2,2,4-trimethylpentane
T=-25.1 - 68.9°C; Irradiationvarious of solvent and temperature, ΔE excit; Thermodynamic dataMechanismRate constant;
参考文献
Griller; Nazran; Scaiano
Journal of the American Chemical Society, 1984 , vol. 106, # 1 p. 198 - 202
反应条件
1: (S)-2-(3,4-Dimethoxy-phenyl)-8-(1,3-diphenyl-propyl)-5,7-dimethoxy-chroman With ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile
T=20°C; Oxidation; 2 h;
2: diphenyldiazo-methane in tetrahydrofuran; methanol
T=20°C; Alkylation; 19.1 h; Further byproducts given;
参考文献
Kozikowski, Alan P.; Tueckmantel, Werner; George, Clifford
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5371 - 5381
反应条件
T=60°C; electrooxidation;
参考文献
Parker, Vernon D.; Bethell, Donald
Journal of the American Chemical Society, 1987 , vol. 109, # 17 p. 5066 - 5072
反应条件
1: 73.5 percent / benzene / Heating
2: 5.3 percent / p-dicyanobenzene (DCB) / acetonitrile / 2 h / 15 °C / Irradiation
View Scheme
参考文献
Tomioka, Hideo; Inoue, Osamu
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 1404 - 1406
反应条件
oxygen in dichloromethane
T=0°C; 0.166667 h; IrradiationRose Bengal ; further dye-sensitizer (Methylene Blue); Product distributionMechanism;
参考文献
Sawaki, Yasuhiko; Kato, Hiroshi; Ogata, Yoshiro
Journal of the American Chemical Society, 1981 , vol. 103, # 13 p. 3832 - 3837
反应条件
λ: 288 nm.Photolysis; Quantum yield;
参考文献
Turro, Nicholas J.; Cha, Yuan; Gould, Ian R.
Tetrahedron Letters, 1985 , vol. 26, # 48 p. 5951 - 5954
反应条件
T=-196.1°C; 0.5 h; Irradiationfurther light intesity, reaction time; Product distribution;
参考文献
Leyva, Elisa; Barcus, Robert L.; Platz, Matthew S.
Journal of the American Chemical Society, 1986 , vol. 108, # 24 p. 7786 - 7788
反应条件
in 2,2,4-trimethylpentane
Irradiation;
参考文献
Turro, Nicholas J.; Cha, Yuan; Gould, Ian R.
Tetrahedron Letters, 1985 , vol. 26, # 48 p. 5951 - 5954