908093-98-1合成路线 （共 442 条）
反应条件
T=0°C; (photolysis);
参考文献
Tomioka,H. et al.
Journal of the American Chemical Society, 1979 , vol. 101, p. 6009 - 6012
反应条件
in solid matrix
T=-196°C; Irradiationtemperature dependence of product distributions; Product distribution;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Journal of the American Chemical Society, 1982 , vol. 104, # 11 p. 3156 - 3162
反应条件
pyridine; water
T=25°C; other rates of solvents; MechanismProduct distribution;
参考文献
McLennan, Duncan J.; Martin, Peter L.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1099 - 1106
反应条件
T=24°C; Irradiationvar. temp., other diazo comp.; Product distribution;
参考文献
Tomioka, Hideo; Miwa, Takaaki; Suzuki, Shinji; Izawa, Yasuji
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 3 p. 753 - 756
反应条件
2: lithium diisopropylamide; diethyl ether / anschliessend Erwaermen mit CH3I
View Scheme
参考文献
Walborsky; Hornyak
Journal of the American Chemical Society, 1955 , vol. 77, p. 6026,6029
反应条件
copper(l) iodide; cesium fluoride in 1,4-dioxane; 1-methyl-pyrrolidin-2-one
T=20°C; 10 h; Glovebox; Reagent/catalystSolvent;
参考文献
Hu, Mingyou; He, Zhengbiao; Gao, Bing; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17302 - 17305
反应条件
1: With copper(l) iodide; cesium fluoride in 1-methyl-pyrrolidin-2-one
T=20°C; 0.5 h; GloveboxSchlenk technique;
2: With water in 1-methyl-pyrrolidin-2-one
0.0833333 h; GloveboxSchlenk technique;
参考文献
Hu, Mingyou; He, Zhengbiao; Gao, Bing; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17302 - 17305
反应条件
in petroleum ether
20°C;
参考文献
Middleton,W.J. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 1375 - 1384
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Gmelin Handbook: F: PerFHalOrg.1, 1.1.1.1, page 1 - 7
反应条件
diethyl ether
anschliessendes Behandeln mit Ammoniak enthaltender wss. Ammoniumchlorid-Loesung;
参考文献
Coleman et al.
Journal of Organic Chemistry, 1938 , vol. 3, p. 99,106
反应条件
in tetrahydrofuran
Ambient temperature;
参考文献
Okuma, Kentaro; Kojima, Kazuki; Ohta, Hiroshi
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 80, # 1-4 p. 259 - 262
