908094-04-2合成路线 （共 238 条）
反应条件
T=0°C; Irradiation; Yield given. Yields of byproduct given;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
反应条件
gold in 1,2-dichloro-ethane
T=20°C; 24 h; Inert atmosphere; optical yield given as percent de;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
反应条件
gold in 1,2-dichloro-ethane
T=80°C; 24 h; Inert atmosphere; optical yield given as percent de;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
反应条件
iodine; diethylzinc in dichloromethane
T=20°C; Simmons-Smith Cyclopropanation; 2.5 h; Inert atmosphere; Overall yield = 71 percent; Overall yield = 69 mg; diastereoselective reaction;
参考文献
Levesque, Eric; Goudreau, Sebastien R.; Charette, Andre B.
Organic Letters, 2014 , vol. 16, # 5 p. 1490 - 1493
反应条件
copper acetylacetonate in 1,2-dichloro-ethane
T=25°C;
参考文献
Berkessel, Albrecht; Kaiser, Patrick; Lex, Johann
Chemistry - A European Journal, 2003 , vol. 9, # 19 p. 4746 - 4756
反应条件
lithium bromide in diethyl ether
T=-5 - 0°C; protected from light;
参考文献
Loeschorn, Carol A.; Nakajima, Masayuki; McCloskey, Patrick J.; Anselme, Jean-Pierre
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4407 - 4410
反应条件
in tetrahydrofuran
Yield given;
参考文献
Dudman, Christopher C.; Reese, Colin B.
Synthesis, 1982 , # 5 p. 419 - 421
反应条件
diethyl ether
unter Ausschluss von H2O und Alkoholen;
参考文献
Eistert; Mueller
Chemische Berichte, 1959 , vol. 92, p. 2071,2073
反应条件
2: diethyl ether
View Scheme
参考文献
Mohrbacher; Cromwell
Journal of the American Chemical Society, 1957 , vol. 79, p. 401,405
反应条件
in tetrahydrofuran; methanol
T=20°C; 1 h; Further byproducts given;
参考文献
Oshima, Takumi; Nagai, Toshikazu
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 3 p. 726 - 730
