908094-04-2合成路线 (共 238 条)
反应条件
in acetone
T=-78 - 23°C; Esterification; decomposition; Product distribution; Further Variations:Temperaturesreaction times;
参考文献
Song, Fenhong; Darbeau, Ron W.; White, Emil H.
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1825 - 1829
反应条件
1: 4-methoxy-aniline With hydrogenchloride; isopentyl nitrite in ethanol
T=0 - 5°C;
2: phenyldiazomethane in ethanol; chloroform; water
T=0 - 20°C; 0.75 h; Further stages.;
参考文献
Butler, Richard N.; Hanniffy, John M.; Stephens, John C.; Burke, Luke A.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1354 - 1364
反应条件
T=-50°C; Irradiationalso diisopropylether and diethylamine; also in the presence of var. additives as Ph2CO, i-PrOH; other temp.; Product distribution;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 492 - 495
反应条件
copper(II) sulfate
T=40°C;
参考文献
Ando,W. et al.
Journal of Organic Chemistry, 1977 , vol. 42, # 21 p. 3365 - 3372
反应条件
scandium tris(trifluoromethanesulfonate) in toluene
T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Wommack, Andrew J.; Moebius, David C.; Travis, Austin L.; Kingsbury, Jason S.
Organic Letters, 2009 , vol. 11, # 15 p. 3202 - 3205
反应条件
scandium tris(trifluoromethanesulfonate) in toluene
T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Wommack, Andrew J.; Moebius, David C.; Travis, Austin L.; Kingsbury, Jason S.
Organic Letters, 2009 , vol. 11, # 15 p. 3202 - 3205
反应条件
[CpFe(CO)2(THF)][BF4] in dichloromethane
T=20°C; Cycloaddition; insertion; 12.5 h;
参考文献
Mahmood, Syed J.; Saha, Anjan K.; Mahmun Hossain
Tetrahedron, 1998 , vol. 54, # 3-4 p. 349 - 358
反应条件
zinc(II) iodide in diethyl ether
2 h; Ambient temperature;
参考文献
Bartnik, R.; Mloston, G.
Acta Chimica Academiae Scientiarum Hungaricae, 1981 , vol. 106, # 4 p. 309 - 312
反应条件
diethyl ether
anschlissendes Behandeln mit Aethanol;
参考文献
Mueller; Disselhoff
Justus Liebigs Annalen der Chemie, 1934 , vol. 512, p. 250,252, 259
反应条件
tetrafluoroboric acid in dichloromethane
T=-40°C; 1 h;
参考文献
Liotta, Louis J.; Ganem, Bruce
Israel Journal of Chemistry, 1991 , vol. 31, # 3 p. 215 - 222