(1-重氮-2-氧代-丙醇)-膦酸二甲酯合成路线 （共 103 条）
反应条件
potassium carbonate in methanol T=20°C; 8 h;
参考文献
Roth, Gerald J.; Liepold, Bernd; Mueller, Stephan G.; Bestmann, Hans Juergen
Synthesis, 2004 , # 1 p. 59 - 62
反应条件
potassium carbonate in methanol T=20°C;
参考文献
Paterson, Ian; Menche, Dirk; Hakansson, Anders E.; Longstaff, Adrian; Wong, David; Barasoain, Isabel; Buey, Ruben M.; Diaz, J. Fernando
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 9 p. 2243 - 2247
反应条件
methanol; potassium carbonate T=0°C;
参考文献
Ohira, Susumu
Synthetic Communications, 1989 , vol. 19, # 3and4 p. 561 - 564
反应条件
methanol; potassium carbonate in methanol 8 h; Inert atmosphere of N2;
参考文献
AKAAL PHARMA PTY LTD; GILL, Gurmit S; GROBELNY, Damian W
Patent: WO2010/43000 A1, 2010 ;
Location in patent: Page/Page column 56 ;
WO 2010/043000 A1
反应条件
potassium carbonate in methanol; dichloromethane T=20°C;
参考文献
Maisonneuve, Stephane; Xie, Juan
Synlett, 2009 , # 18 p. 2977 - 2981
反应条件
potassium carbonate in methanol 3 h;
参考文献
Braisted, Andrew C.; Oslob, Johan D.; Delano, Warren L.; Hyde, Jennifer; McDowell, Robert S.; Waal, Nathan; Yu, Chul; Arkin, Michelle R.; Raimundo, Brian C.
Journal of the American Chemical Society, 2003 , vol. 125, # 13 p. 3714 - 3715
反应条件
potassium tert-butylate in methanol T=100°C; 0.5 h;
参考文献
Baxendale, Ian R.; Ley, Steven V.; Mansfield, Andrew C.; Smith, Christopher D.
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 4017 - 4021
Angewandte Chemie, 2009 , vol. 121, p. 4077 - 4081
反应条件
potassium carbonate in methanol T=0 - 20°C;
参考文献
Organic Letters, , vol. 12, # 7 p. 1580 - 1583
反应条件
potassium carbonate in methanol T=20°C; BESTMANN-OHIRA reaction; 12 h;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; STEURER, Steffen; ETTMAYER, Peter; MANTOULIDIS, Andreas
Patent: WO2011/117381 A1, 2011 ;
Location in patent: Page/Page column 52-53 ;
WO 2011/117381 A1
反应条件
potassium tert-butylate in methanol T=100°C; 0.5 h;
参考文献
Baxendale, Ian R.; Ley, Steven V.; Mansfield, Andrew C.; Smith, Christopher D.
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 4017 - 4021
Angewandte Chemie, 2009 , vol. 121, p. 4077 - 4081
