反应条件
in tetrahydrofuran; diethyl ether mixture of PhMgBr and Sb-compound is stirred at -70°C; the soln. was made basic with concd. NaOH, (CH3O)2SO2 was added at 5°C, heating to 70°C for 15 min, further products: octamethylcyclotetrasiloxane, α-methylbenzenemethanol; VPC-analysis;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 36, p. 153 - 164
