反应条件
in tetrahydrofuran byproducts: NaCl; absence of air and moisture; slow addn. of 1 equiv. Ga-compd. to naphthalenide soln. (prepd. by stirring equimolar amts. of Na and naphthalenefor 18 h), stirring (-78°C, 18 h), slow warming to room temp., stirring for 14-19 h; solvent removal (vac.), extn. into C6H6, chromy. (Bio-Beads), recrystn.(pentane/C6H6=5:1 v/v); elem. anal.;
参考文献
Beachley Jr.; Noble, Matthew J.; Allendoerfer, Robert D.
Journal of Organometallic Chemistry, 1999 , vol. 582, # 1 p. 32 - 39
