2,4-二甲氧基苯甲酸合成路线 （共 127 条）
反应条件
Pd(OTf)2; silver carbonate in dimethyl sulfoxide; N,N-dimethyl-formamide T=100°C;
参考文献
Ouchaou, Kahina; Georgin, Dominique; Taran, Frederic
Synlett, 2010 , # 14 art. no. G18110ST, p. 2083 - 2086
反应条件
Pd(OTf)2; silver carbonate in dimethyl sulfoxide; N,N-dimethyl-formamide 0.0166667 h;
参考文献
Ouchaou, Kahina; Georgin, Dominique; Taran, Frederic
Synlett, 2010 , # 14 art. no. G18110ST, p. 2083 - 2086
反应条件
Pd(TFA)2; silver carbonate; tri-cyclo-hexyl-phosphine in ethylene glycol dimethyl ether; dimethyl sulfoxide T=120°C; 24 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 24 p. 5945 - 5949
反应条件
Pd(TFA)2; silver carbonate; tri-cyclo-hexyl-phosphine in 1,4-dioxane; dimethyl sulfoxide T=120°C; 24 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 24 p. 5945 - 5949
反应条件
Pd(TFA)2; triphenylphosphine; silver carbonate in ethylene glycol dimethyl ether; dimethyl sulfoxide T=120°C; 24 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 24 p. 5945 - 5949
反应条件
Pd(TFA)2; silver carbonate in 1-methyl-pyrrolidin-2-one T=120°C; 24 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 24 p. 5945 - 5949
反应条件
1: phosphorus (V)-chloride 2: aqueous ammonia View Scheme
参考文献
Pfeiffer; Breitbach; Scholl
Journal fuer Praktische Chemie (Leipzig), 1940 , vol. <2> 154, p. 157,195
反应条件
PPA in methoxybenzene
参考文献
Corning S.A.
Patent: EP1038870 A1, 2000 ;
反应条件
lithium aluminium tetrahydride; thionyl chloride
参考文献
Shepard et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 568,570
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran 0.0833333 h; Ambient temperature;
参考文献
McGeary, Ross P.
Tetrahedron Letters, 1998 , vol. 39, # 20 p. 3319 - 3322
