2,4-二甲氧基苯甲酸合成路线 (共 127 条)
参考文献
Genzyme Corporation
Patent: US2003/220504 A1, 2003 ;
Location in patent: Page/Page column 3 ;
反应条件
aluminium trichloride in chlorobenzene 0.75 h; Heating;
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
[VO((R,R)-N,N-disalicylidenecyclohexane-1,2-diamine-2H)(methanol)]ClO4; dihydrogen peroxide; potassium bromide in acetonitrile T=60 - 80°C; 12 h; High-pressure reactor;
参考文献
Si, Tapan Kumar; Drew, Michael G.B.; Mukherjea, Kalyan Kumar
Polyhedron, 2011 , vol. 30, # 13 p. 2286 - 2293
反应条件
bromine; acetic acid
参考文献
Iyengar; Jois
J. Mysore Univ., 1931 , vol. 5, p. 232
参考文献
Iyengar; Jois
J. Mysore Univ., 1931 , vol. 5, p. 232
反应条件
bromine; acetic acid
参考文献
Iyengar; Jois
J. Mysore Univ., 1931 , vol. 5, p. 232
参考文献
Iyengar; Jois
J. Mysore Univ., 1931 , vol. 5, p. 232
反应条件
1: With palladium (II) trifluoroacetate; 6-mbipy in water T=130°C; 1 h; Microwave irradiation; 2: With formic acid in water T=100°C; 1 h;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 42 p. 7733 - 7737
反应条件
1: palladium (II) trifluoroacetate; 6-mbipy; p-benozquinone / N,N-dimethyl-formamide / 24 h / 120 °C 2: hydrogenchloride; water / 2 h / 20 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 356, # 4 p. 870 - 878
反应条件
1: 59 percent / bromine / CHCl3 / 5 h / Ambient temperature 2: 43 percent / boron tribromide / CH2Cl2 / 1 h / 10 °C View Scheme
参考文献
De Paulis; Hall; Kumar; Ramsby; Ogren; Hogberg
European Journal of Medicinal Chemistry, 1990 , vol. 25, # 6 p. 507 - 517