3-羟基-N,N-二乙基苯胺合成路线 （共 78 条）
反应条件
sodium hydroxide 2 h;
参考文献
Pirrung; Fallon; Zhu; Yong Rok Lee
Journal of the American Chemical Society, 2001 , vol. 123, # 16 p. 3638 - 3643
反应条件
water; potassium hydrogencarbonate unter Durchleiten von CO2;
参考文献
Doub et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 903,904
反应条件
1: 2-amino-6-methyl-benzothiazole With sulfuric acid; acetic acid; sodium nitrite in water T=-5°C; 2: N,N-diethyl-m-aminophenol in methanol; water T=0 - 5°C; 2.5 h;
参考文献
Tao, Tao; Xu, Feng; Chen, Xiao-Chun; Liu, Qian-Qian; Huang, Wei; You, Xiao-Zeng
Dyes and Pigments, 2012 , vol. 92, # 3 p. 916 - 922
反应条件
triethylamine in tetrahydrofuran 1 h;
参考文献
Cegan; Vecere
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 5 p. 1440 - 1446
反应条件
1.1: toluene / Reflux 2.1: methanesulfonic acid / 24 h / 20 - 25 °C 2.2: 4 h / 75 - 80 °C View Scheme
参考文献
Azizian, Farid; Field, Amanda J.; Griffiths, John; Heron, B. Mark
Dyes and Pigments, 2012 , vol. 92, # 1 p. 524 - 530
反应条件
1.1: toluene / Reflux 2.1: sulfuric acid / 4 h / 120 - 125 °C 2.2: 0.5 h / Reflux 3.1: tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; [(t-Bu)3PH]BF4 / toluene / 24 h / 70 °C / Inert atmosphere View Scheme
参考文献
Azizian, Farid; Field, Amanda J.; Griffiths, John; Heron, B. Mark
Dyes and Pigments, 2012 , vol. 92, # 1 p. 524 - 530
反应条件
titanium tetrachloride in tetrahydrofuran Heating;
参考文献
Bissell
Synthesis, 1982 , vol. No. 10, p. 846 - 848
反应条件
1: 93 percent / Et3N / CCl4 2: 61 percent / 4,4'-di-tert-butylbiphenyl lithium / tetrahydrofuran / 2 h / 0 °C View Scheme
参考文献
Lusch, Michael J.; Woller, Kevin R.; Keller, Anthony M.; Turk, Michael C.
Synthesis, 2005 , # 4 art. no. M06904SS, p. 551 - 554
反应条件
1: 89 percent / 0.08 h / Heating 2: 1) piperidine, 2) conc. HCl / 1) ethanol, reflux, 2) aq. ethanol, heating View Scheme
参考文献
Czerney, P.; Hartmann, H.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 1 p. 21 - 28
反应条件
in toluene 8 h; Reflux;
参考文献
Bochkov, Andrei Y.; Akchurin, Igor O.; Dyachenko, Oleg A.; Traven, Valery F.
Chemical Communications, 2013 , vol. 49, # 99 p. 11653 - 11655
