1.1: magnesium / diethyl ether 1.2: 74 percent / diethyl ether / 0 - 20 °C 2.1: 77 percent / chromium(VI) oxide; Celite / pyridine / 8 h / 20 °C 3.1: 73 percent / p-toluenesulfonic acid monohydrate; trimethyl orthoformate / 12 h / 20 °C 4.1: 82 percent / EtAlCl2 / CH2Cl2 / 1 h / -78 - 20 °C 5.1: 71 percent / methyltrioctylammonium chloride; KMnO4 / benzene; H2O / 1.5 h / 0 - 45 °C 6.1: 67 percent / acetic anhydride / 8 h / Heating 7.1: 94 percent / DDQ / dioxane / 5 h / Heating View Scheme

1: 73 percent / p-toluenesulfonic acid monohydrate; trimethyl orthoformate / 12 h / 20 °C 2: 82 percent / EtAlCl2 / CH2Cl2 / 1 h / -78 - 20 °C 3: 71 percent / methyltrioctylammonium chloride; KMnO4 / benzene; H2O / 1.5 h / 0 - 45 °C 4: 67 percent / acetic anhydride / 8 h / Heating 5: 94 percent / DDQ / dioxane / 5 h / Heating View Scheme

1: 71 percent / methyltrioctylammonium chloride; KMnO4 / benzene; H2O / 1.5 h / 0 - 45 °C 2: 67 percent / acetic anhydride / 8 h / Heating 3: 94 percent / DDQ / dioxane / 5 h / Heating View Scheme

1: 67 percent / acetic anhydride / 8 h / Heating 2: 94 percent / DDQ / dioxane / 5 h / Heating View Scheme

1: 77 percent / chromium(VI) oxide; Celite / pyridine / 8 h / 20 °C 2: 73 percent / p-toluenesulfonic acid monohydrate; trimethyl orthoformate / 12 h / 20 °C 3: 82 percent / EtAlCl2 / CH2Cl2 / 1 h / -78 - 20 °C 4: 71 percent / methyltrioctylammonium chloride; KMnO4 / benzene; H2O / 1.5 h / 0 - 45 °C 5: 67 percent / acetic anhydride / 8 h / Heating 6: 94 percent / DDQ / dioxane / 5 h / Heating View Scheme

1: 82 percent / EtAlCl2 / CH2Cl2 / 1 h / -78 - 20 °C 2: 71 percent / methyltrioctylammonium chloride; KMnO4 / benzene; H2O / 1.5 h / 0 - 45 °C 3: 67 percent / acetic anhydride / 8 h / Heating 4: 94 percent / DDQ / dioxane / 5 h / Heating View Scheme

hydrogenchloride; acetic acid

hydrogenchloride; acetic acid

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