Oyaizu, Kenichi; Haryono, Agus; Natori, Junichiro; Shinoda, Hiroshi; Tsuchida, Eishun
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 5 p. 1153 - 1163
in N,N-dimethyl-formamide tetraphenylporphyrin and excess iron chloride refluxed in DMF for 4 h, cooled on ice bath, cold water added to soln. and complex ppd.; FTIR, UV-vis, 1H NMR;
参考文献
Costa, Andreia A.; Ghesti, Grace F.; de Macedo, Julio L.; Braga, Valdeilson S.; Santos, Marcello M.; Dias, Jose A.; Dias, Silvia C.L.
Journal of Molecular Catalysis A: Chemical, 2008 , vol. 282, # 1-2 p. 149 - 157
in chloroform; acetic acid addn. of NaCl to soln. of tetraphenylporphyrin in CHCl3; filtration of hot glacial acetic acid satd. with iron(II) acetate (prepared by dissolving Fe powder in boiling glacial acid) into this soln.; refluxing soln. for 2 h; concg.; cooling; filtration;; extraction in Soxhlet apparatus with CHCl3; concg. soln.; addn. of hot methanol; cooling; pptn.;;
参考文献
Sheng, Tai-Cheng; Rebenstorf, Bernd; Wideloev, Anders; Larsson, Ragnar
Journal of the Chemical Society, Faraday Transactions, 1992 , vol. 88, # 3 p. 477 - 482
in toluene
byproducts: H2; cocondensation of iron and toluene vapor at liq. nitrogen temp.; heating to -94.6°C; dropwise addn. of porphine soln. under nitrogen to the slurry (molar ratio Fe:porphine 4:1); gradually warming to 0°C, 1h; filtration; evapn. of filtrate;
参考文献
Reagen, William K.; Radonovich, Lewis J.
Journal of the American Chemical Society, 1987 , vol. 109, p. 5274 - 5275
Collman, James P.; Basolo, Fred; Bunnenberg, Edward; Collins, Terrence J.; Dawson, John H.; et al.
Journal of the American Chemical Society, 1981 , vol. 103, # 19 p. 5636 - 5648
