反应条件
in tetrahydrofuran; diethyl ether; n-heptane
Ar atmosphere, addn. of (C4H9)2AlH to pyrrolidine, Si compd. addn. (55°C), evapn., cooling (-78°C, Et2O), warming (0°C), MeLi addn. (Et2O, 20°C), addn. Cu complex and Me3SnCl-further educt (THF, -78°C), extn. (Et2O); washing (water), drying, addn. of hexane, filtration, chromy. (silica gel, hexane); elem. anal.;
参考文献
Rossi, Renzo; Carpita, Adriano; Bellina, Fabio; De Santis, Massimo; Veracini, Carlo Alberto
Gazzetta Chimica Italiana, 1990 , vol. 120, p. 457 - 464
