1: methyllithium With titanium tetrachloride in diethyl ether T=-80°C; 0.25 h; 2: indan-2-one in diethyl ether T=-50 - 20°C; 3: With water in diethyl ether
参考文献
Doherty, Elizabeth M.; Katon, Jodie; Norman, Mark H.; Retz, Daniel M.; Wang, Xianghong; Bo, Yunxin Y.; Tamayo, Nuria; Nishimura, Nobuko; Liao, Hongyu
Patent: US2006/241296 A1, 2006 ;
Location in patent: Page/Page column 63 ;
US 20060241296 A1
1: methyllithium With indium(III) chloride in tetrahydrofuran T=-78 - 20°C; 2: 4-tert-butyl-1-cyclohexen-1-yl trifluoromethanosulfonate With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 7 h; Heating; Further stages.;
参考文献
Perez, Ignacio; Sestelo, Jose Perez; Sarandeses, Luis A.
Organic Letters, 1999 , vol. 1, # 8 p. 1267 - 1269
