in diethyl ether; pentane
addn. of soln. of Me3SnCl to soln. of Li-compound (prepd. in situ) at -120°C, warming to room temp.; shaking with water, drying and concn. of org. phase; anal. and GC;
参考文献
Eikema Hommes, Nicolaas J. R.; Bickelhaupt, Friedrich; Klumpp, Gerhard W.
Angewandte Chemie, 1988 , vol. 100, # 8 p. 1100 - 1107
Bergel'son,L.D.; Grigoryan,A.N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1966 , p. 256 - 257
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , p. 286 - 289