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乙二醇
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63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
917947-75-2
合成路线
（共 7 条）
77169-12-1
1,3-二苯基-1H-吡唑-4-羧酸
+
613-94-5
苯甲酰肼
→
反应条件
917947-75-2
反应条件
trichlorophosphate 2 h; Reflux;
参考文献
Xia, Qingchun; Xu, Dongfang; He, Qizhuang; Li, Xingyu; Sun, Dazhi
Chinese Journal of Chemistry, 2010 , vol. 28, # 12 p. 2433 - 2440
65-85-0
苯甲酸
→
反应条件
917947-75-2
反应条件
1: sulfuric acid / 12 h / |Reflux 2: hydrazine hydrate / ethanol / 16 h / |Reflux 3: acetic acid / ethanol / 4 h / |Reflux 4: [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C View Scheme
参考文献
Bansal, Sumit; Bala, Manju; Suthar, Sharad Kumar; Choudhary, Shivani; Bhattacharya, Shoumyo; Bhardwaj, Varun; Singla, Sumit; Joseph, Alex
European Journal of Medicinal Chemistry, 2014 , vol. 80, p. 167 - 174
93-58-3
苯酸甲酯
→
反应条件
917947-75-2
反应条件
1: hydrazine hydrate / ethanol / 16 h / |Reflux 2: acetic acid / ethanol / 4 h / |Reflux 3: [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C View Scheme
参考文献
Bansal, Sumit; Bala, Manju; Suthar, Sharad Kumar; Choudhary, Shivani; Bhattacharya, Shoumyo; Bhardwaj, Varun; Singla, Sumit; Joseph, Alex
European Journal of Medicinal Chemistry, 2014 , vol. 80, p. 167 - 174
583-11-9
苯乙酮苯腙
→
反应条件
917947-75-2
反应条件
1.1: trichlorophosphate / 1.5 h / 0 °C 1.2: 6 h / 0 - 20 °C / |Reflux 2.1: acetic acid / ethanol / 4 h / |Reflux 3.1: [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C View Scheme
参考文献
Bansal, Sumit; Bala, Manju; Suthar, Sharad Kumar; Choudhary, Shivani; Bhattacharya, Shoumyo; Bhardwaj, Varun; Singla, Sumit; Joseph, Alex
European Journal of Medicinal Chemistry, 2014 , vol. 80, p. 167 - 174
98-86-2
苯乙酮
→
反应条件
917947-75-2
反应条件
1.1: acetic acid / ethanol / 1 h / |Reflux 2.1: trichlorophosphate / 1.5 h / 0 °C 2.2: 6 h / 0 - 20 °C / |Reflux 3.1: acetic acid / ethanol / 4 h / |Reflux 4.1: [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C View Scheme
参考文献
Bansal, Sumit; Bala, Manju; Suthar, Sharad Kumar; Choudhary, Shivani; Bhattacharya, Shoumyo; Bhardwaj, Varun; Singla, Sumit; Joseph, Alex
European Journal of Medicinal Chemistry, 2014 , vol. 80, p. 167 - 174
100-63-0
苯肼
→
反应条件
917947-75-2
反应条件
1.1: acetic acid / ethanol / 1 h / |Reflux 2.1: trichlorophosphate / 1.5 h / 0 °C 2.2: 6 h / 0 - 20 °C / |Reflux 3.1: acetic acid / ethanol / 4 h / |Reflux 4.1: [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C View Scheme
参考文献
Bansal, Sumit; Bala, Manju; Suthar, Sharad Kumar; Choudhary, Shivani; Bhattacharya, Shoumyo; Bhardwaj, Varun; Singla, Sumit; Joseph, Alex
European Journal of Medicinal Chemistry, 2014 , vol. 80, p. 167 - 174
613-94-5
苯甲酰肼
+
21487-45-6
1,3-二苯-1H-吡唑-4-甲醛
→
反应条件
917947-75-2
反应条件
1: acetic acid / ethanol / 4 h / |Reflux 2: [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C View Scheme
参考文献
Bansal, Sumit; Bala, Manju; Suthar, Sharad Kumar; Choudhary, Shivani; Bhattacharya, Shoumyo; Bhardwaj, Varun; Singla, Sumit; Joseph, Alex
European Journal of Medicinal Chemistry, 2014 , vol. 80, p. 167 - 174
