N-叔丁基-4-(三氟甲基)苯甲酰胺合成路线 (共 7 条)
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane T=170°C; 1 h; Irradiation;
参考文献
Mahalingam; Wu, Xiongyu; Alterman, Mathias
Tetrahedron Letters, 2006 , vol. 47, # 18 p. 3051 - 3053
反应条件
sulfuric acid in acetic acid
T=20°C; Ritter reaction; 2.5 h; Inert atmosphere;
参考文献
Baum, Jean C.; Milne, Jacqueline E.; Murry, Jerry A.; Thiel, Oliver R.
Journal of Organic Chemistry, 2009 , vol. 74, # 5 p. 2207 - 2209
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
in dichloromethane; benzene
参考文献
Centaur Pharmaceuticals, Inc.
Patent: US6271265 B1, 2001 ;
反应条件
air; 1,8-diazabicyclo[5.4.0]undec-7-ene; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in tetrahydrofuran
T=150°C; 0.25 h;
参考文献
Wannberg, Johan; Larhed, Mats
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5750 - 5753
反应条件
bismuth trifluoromethanesulphonate; water in nitrobenzene
Ritter reaction;
参考文献
Callens, Emmanuel; Burton, Andrew J.; Barrett, Anthony G.M.
Tetrahedron Letters, 2006 , vol. 47, # 49 p. 8699 - 8701
反应条件
air
Ambient temperature;
参考文献
Auret, Barbara J.; Boyd, Derek R.; Coulter, Peter B.
Journal of the Chemical Society, Chemical Communications, 1984 , # 7 p. 463 - 464