1: 2,2,2-trifluoroethyl(dimethylphosphonyl) acetate With sodium hydride in tetrahydrofuran
T=0°C; 0.166667 h;
2: (E)-cinnamaldehyde in tetrahydrofuran
T=-78°C; Horner-Wadsworth-Emmons reaction; 90 h; Further stages. Title compound not separated from byproducts.;