反应条件
1: cyclohexanone With N,N'-dimethyl-N,N'-propyleneurea; lithium diisopropyl amide in tetrahydrofuran; hexane
T=-78°C; 0.75 h;
2: 1-bromo-2-(bromomethyl)benzene in tetrahydrofuran; hexane
T=-78°C; 2 h; Further stages.;
参考文献
Kelly, Sean A.; Foricher, Yann; Mann, John; Bentley, Jonathan M.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 16 p. 2865 - 2876