反式-2-已烯-1-醇合成路线 （共 129 条）
反应条件
4-methyl-pyridin-2-ylamine; benzoic acid; RhCl(PPh3)3
T=130°C; 4 h;
参考文献
Lee, Dae-Yon; Moon, Choong Woon; Jun, Chul-Ho
Journal of Organic Chemistry, 2002 , vol. 67, # 11 p. 3945 - 3948
反应条件
in neat (no solvent)
T=50°C; P=750.075 Torr; 24 h; Green chemistry; Reagent/catalyst;
参考文献
Alshammari, Hamed; Miedziak, Peter J.; Morgan, David J.; Knight, David W.; Hutchings, Graham J.
Green Chemistry, 2013 , vol. 15, # 5 p. 1244 - 1254
反应条件
in neat (no solvent)
T=50°C; P=750.075 Torr; 24 h; Green chemistry; Reagent/catalyst;
参考文献
Alshammari, Hamed; Miedziak, Peter J.; Morgan, David J.; Knight, David W.; Hutchings, Graham J.
Green Chemistry, 2013 , vol. 15, # 5 p. 1244 - 1254
反应条件
in neat (no solvent)
T=50°C; P=750.075 Torr; 24 h; Green chemistry; Reagent/catalyst;
参考文献
Alshammari, Hamed; Miedziak, Peter J.; Morgan, David J.; Knight, David W.; Hutchings, Graham J.
Green Chemistry, 2013 , vol. 15, # 5 p. 1244 - 1254
反应条件
potassium cyanide; potassium hydroxide; potassium chloride; hydrogen; β-cyclodextrin; cobalt(II) chloride
24 h;
参考文献
Lee, Jong-Tae; Alper, Howard
Tetrahedron Letters, 1990 , vol. 31, # 29 p. 4101 - 4104
反应条件
1: 79 percent / pyridine / 3 h / Ambient temperature
2: 7 percent Spectr. / PdCl2(dppf) (dppf=(CpPPh2)2Fe) / diethyl ether / 20 h / Ambient temperature
View Scheme
参考文献
Kiuchi, Hiroyoshi; Takahashi, Dai; Funaki, Kenji; Sato, Tetsuo; Oi, Shuichi
Organic Letters, 2012 , vol. 14, # 17 p. 4502 - 4505
反应条件
1: 88 percent / sodium hydride / tetrahydrofuran / 18 h / 20 °C
2: chiral palladim(II)-based complex; diisopropylethylamine / CH2Cl2 / 30 h / 20 °C
View Scheme
参考文献
Overman, Larry E; Owen, Carolyn E; Pavan, Mary M; Richards, Christopher J
Organic letters, 2003 , vol. 5, # 11 p. 1809 - 1812
反应条件
sodium hydride in N,N-dimethyl-formamide; mineral oil
T=20°C; 2 h;
参考文献
Park, Sae Rom; Kim, Cheoljae; Kim, Dong-Gil; Thrimurtulu, Neetipalli; Yeom, Hyun-Suk; Jun, Jungho; Shin, Seunghoon; Rhee, Young Ho
Organic Letters, 2013 , vol. 15, # 6 p. 1166 - 1169
反应条件
With tert.-butylhydroperoxide in chloroform 4 h; Reflux; Catalytic behavior;
参考文献
Hamidipour, Lida; Farzaneh, Faezeh Comptes Rendus Chimie, 2014 , vol. 17, # 9 p. 927 - 933
反应条件
With magnesium iodide in benzene T=80°C; 3 h;
参考文献
Martinez, Antonio Garcia; Villalobos, Angeles Cruces; Ruiz, Manuel Oliver Synthesis, 1988 , # 1 p. 58 - 60
