反式-2-已烯-1-醇合成路线 (共 129 条)
反应条件
With triphenylphosphine; diethylazodicarboxylate in dichloromethane; toluene T=0 - 20°C; Mitsunobu reaction;
参考文献
Jeon, Jae-Ho; Kim, Mi Ran; Jun, Jong-Gab Synthesis, 2011 , # 3 art. no. F18510SS, p. 370 - 376
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '14638110', constants.ctx, '0')">phosphomolybdic acid</a>; <a href="#" onclick="return RXDsubstances(event, this, '3902804', constants.ctx, '0')">silica gel</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=20°C; 0.5 h; <br />
参考文献
Kishore Kumar; Baskaran, Sundarababu Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4520 - 4523
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '11342962', constants.ctx, '0')">tellurium</a>; <a href="#" onclick="return RXDsubstances(event, this, '4151240', constants.ctx, '0')">lithium triethylborohydride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=0°C; 0.2 h; <br />
参考文献
Dittmer, Donald C.; Zhang, Yanzhi; Discordia, Robert P. Journal of Organic Chemistry, 1994 , vol. 59, # 5 p. 1004 - 1010
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '11460447', constants.ctx, '0')">lithium aluminium tetrahydride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />5 h; Heating; <br />
参考文献
Vig, O. P.; Jindal, R. T. Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 919 - 920
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '11343078', constants.ctx, '0')">sodium tetrahydroborate</a>; <a href="#" onclick="return RXDsubstances(event, this, '9802819', constants.ctx, '0')">erbium trifluoromethanesulfonate</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102448', constants.ctx, '0')">2-methyl tetrahydrofuran</a> <br />T=20°C; 0.0833333 h; Green chemistry; regioselective reaction; <br /> <br />
参考文献
Nardi, Monica; Sindona, Giovanni; Costanzo, Paola; Oliverio, Manuela; Procopio, Antonio Tetrahedron, 2015 , vol. 71, # 7 p. 1132 - 1135
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '15594225', constants.ctx, '0')">bis(cyclopentadienyl)zirconium dihydride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '635639', constants.ctx, '0')">isopropyl alcohol</a> <br />T=130°C; 8 h; <br />
参考文献
Nakano, Tatsuya; Umano, Shigetoshi; Kino, Yoshio; Ishii, Yasutaka; Ogawa, Masaya Journal of Organic Chemistry, 1988 , vol. 53, # 16 p. 3752 - 3757
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '4123663', constants.ctx, '0')">diisobutylaluminium hydride</a> <br />T=0 - 20°C; <br />
参考文献
Srinivas; Sai Pavan Kumar; China Raju; Jayathirtha Rao; Naidu; Ramakrishna; Diwan, Prakash V. Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 20 p. 5915 - 5918
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '3587191', constants.ctx, '0')">dihydrogen peroxide</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '103233', constants.ctx, '0')">pyridine</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=20°C; <br />
参考文献
Giamberardino, T. Di; Halazy, S.; Dumont, W.; Krief, A. Tetrahedron Letters, 1983 , vol. 24, # 32 p. 3413 - 3416
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1446024', constants.ctx, '0')">methanesulfonic acid</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br />T=20°C; 12 h; <br />
参考文献
Leleti, Rajender Reddy; Hu, Bin; Prashad, Mahavir; Repic, Oljan Tetrahedron Letters, 2007 , vol. 48, # 48 p. 8505 - 8507