反式-2-已烯-1-醇合成路线 (共 129 条)
反应条件
pyridinium p-toluenesulfonate in butanone 11 h; Heating;
参考文献
Monti, H.; Leandri, G.; Klos-Ringuet, M.; Corriol, C.
Synthetic Communications, 1983 , vol. 13, # 12 p. 1021 - 1026
反应条件
potassium hydroxide; tetrafluoroboric acid; sodium hydrogencarbonate; mercury(II) oxide in 1,4-dioxane 1.) room temp., 2 h;
参考文献
Barluenga, Jose; Alonso-Cires, Luisa; Campos, Pedro J.; Asensio, Gregorio
Synthesis, 1983 , # 1 p. 53 - 55
反应条件
hydrogen in isopropyl alcohol T=129.84°C; P=22502.3 Torr; 2 h; chemoselective reaction;
参考文献
Rodiansono; Hara, Takayoshi; Ichikuni, Nobuyuki; Shimazu, Shogo
Chemistry Letters, 2012 , vol. 41, # 8 p. 769 - 771
反应条件
1: With potassium hexamethylsilazane in tetrahydrofuran; benzene T=-78 - 20°C; 2 h; 2: With pyridine hydrogenfluoride in tetrahydrofuran; benzene T=0 - 20°C;
参考文献
Organic Letters, , vol. 8, # 26 p. 5983 - 5986
反应条件
lithium aluminium tetrahydride
参考文献
Journal of the American Chemical Society, , vol. 73, p. 2366
Yakugaku Zasshi, , vol. 78, p. 258
Chem.Abstr., , p. 11740
Journal of the Chemical Society, , p. 1770,1774
反应条件
O,O'-(R)-(1,1'-dinaphthyl-2,2'-diyl)-N,N'-di-(R,R)-1-phenylethylphosphoramidite; copper(II) bis(trifluoromethanesulfonate) in toluene T=-78 - 0°C; 5 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 69, # 6 p. 2099 - 2105
反应条件
diisobutylaluminium hydride in diethyl ether T=-78°C;
参考文献
Chemische Berichte, , vol. 119, # 7 p. 2178 - 2190
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=-78°C; 60 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 21 p. 1013 - 1014
反应条件
1: 92 percent / triethylamine, (N,N-dimethylamino)pyridine / CH2Cl2 / Ambient temperature 2: 70 percent / Te, LiEt3BH / tetrahydrofuran / 0.2 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 59, # 5 p. 1004 - 1010
反应条件
copper(l) iodide; lithium aluminium tetrahydride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=-78°C; 60 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 21 p. 1013 - 1014