反式-2-已烯-1-醇合成路线 （共 129 条）
反应条件
cobalt(II) chloride T=60°C; 18 h;
参考文献
Velusamy, Subbarayan; Borpuzari, Sarbani; Punniyamurthy
Tetrahedron, 2005 , vol. 61, # 8 p. 2011 - 2015
反应条件
in dichloromethane 1.) 0 deg C, 2.) room temperature, 1 h;
参考文献
Strazzolini, Paolo; Giumanini, Angelo G.; Verardo, Giancarlo
Tetrahedron, 1994 , vol. 50, # 1 p. 217 - 254
反应条件
1: 62 percent / MgI2 / benzene / 3 h / 80 °C 2: dimethylformamide / 12 h / Ambient temperature View Scheme
参考文献
Martinez, Antonio Garcia; Villalobos, Angeles Cruces; Ruiz, Manuel Oliver
Synthesis, 1988 , # 1 p. 58 - 60
反应条件
n-butyllithium; [Rh(dppe)(NBD)]ClO4 1.) THF, hexane, reflux, 6 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
反应条件
chloro-trimethyl-silane; water; sodium iodide in acetonitrile 0.5 h; Ambient temperature;
参考文献
Kanai, Takaya; Irifune, Shinji; Ishii, Yasutaka; Ogawa, Masaya
Synthesis, 1989 , # 4 p. 283 - 286
反应条件
magnesium iodide in benzene T=80°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Loiseau, Francois; Kholod, Inga; Neier, Reinhard
European Journal of Organic Chemistry, 2010 , # 24 p. 4642 - 4661
反应条件
tin; chloro-trimethyl-silane; water; sodium iodide multistep reaction; other reagents, other aldehydes, other allylic alcohols; Mechanism;
参考文献
Kanagawa, Yoshinori; Nishiyama, Yutaka; Ishii, Yasutaka
Journal of Organic Chemistry, 1992 , vol. 57, # 25 p. 6988 - 6991
反应条件
1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 1 h / 0 °C / Inert atmosphere 2: tetrahydrofuran / 0.25 h / -20 °C / Inert atmosphere View Scheme
参考文献
Radha Krishna, Palakodety; Ramana, D. Venkata
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 674 - 679
反应条件
Lanthanum nitrate hexahydrate T=20°C; 3 h;
参考文献
Reddy, T. Srikanth; Ravinder; Suryakiran; Narasimhulu; Mahesh, K. Chinni; Venkateswarlu
Tetrahedron Letters, 2006 , vol. 47, # 14 p. 2341 - 2344
反应条件
1: 43 percent / HCl (gas) / benzene / 2.5 h / below 15 deg C 2: 83 percent / tetrahydrofuran; dimethylformamide View Scheme
参考文献
Bedford; Harris III; Howd; Goff; Koolpe; Petesch; Koplovitz; Sultan; Musallam
Journal of Medicinal Chemistry, 1989 , vol. 32, # 2 p. 504 - 516
