1,8-二氨基-3,6-二氧杂辛烷合成路线 （共 65 条）
参考文献
Luk'yanenko, N. G.; Bogat-skii, A. V.; Shapkin, V. A.; Popkov, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 944 - 950
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 5 p. 1069 - 1077
反应条件
in ethanol
20 h; Heating;
参考文献
Lukyanenko, N. G.; Bogatsky, A. V.; Kirichenko, T. I.; Scherbakov, S. V.; Nazarova, N. Yu.
Synthesis, 1984 , # 2 p. 137
反应条件
1: 20 percent / ethanol / 20 h / Heating
2: 82 percent / 50percent aq. NaOH / benzyltriethylammonium chloride / 6 h / Heating
View Scheme
参考文献
Lukyanenko, N. G.; Bogatsky, A. V.; Kirichenko, T. I.; Scherbakov, S. V.; Nazarova, N. Yu.
Synthesis, 1984 , # 2 p. 137
反应条件
triethylamine in N,N-dimethyl-formamide
参考文献
Choi, Youngseon; Lee, Junghan; Kim, Keumhyun; Kim, Heeyeon; Sommer, Peter; Song, Rita
Chemical Communications, 2010 , vol. 46, # 48 p. 9146 - 9148
反应条件
TEA in dichloromethane
T=20°C; 4 h;
参考文献
Ha, Tai Hwan; Jung, Sun Ok; Lee, Jeong Min; Lee, Kun Yeong; Lee, Yan; Park, Jong Sang; Chung, Bong Hyun
Analytical Chemistry, 2007 , vol. 79, # 2 p. 546 - 556
反应条件
in dichloromethane
T=-78°C; 13 h;
参考文献
New York University
Patent: US2006/293325 A1, 2006 ;
Location in patent: Page/Page column 10 ;
反应条件
in water
T=50°C; 24 h;
参考文献
Pappas, Kyrie; Zhang, Xiang; Tang, Wei; Fang, Shiyue
Tetrahedron Letters, 2009 , vol. 50, # 41 p. 5741 - 5743
参考文献
Tang, Wei; Fang, Shiyue
Tetrahedron Letters, 2008 , vol. 49, # 41 p. 6003 - 6006
反应条件
in dichloromethane
T=4 - 20°C; Inert atmosphere;
参考文献
Suwal, Sujit; Senevirathne, Chamara; Garre, Satish; Pflum, Mary Kay H.
Bioconjugate Chemistry, 2012 , vol. 23, # 12 p. 2386 - 2391
反应条件
1: 30 percent / acetonitrile / 18 h / Heating
2: 87 percent / dicyklohexylcarbodiimid / CH2Cl2 / 20 h / 20 °C
3: 91 percent / palladium / methanol
View Scheme
参考文献
Luk'yanenko, N. G.; Bogat-skii, A. V.; Basok, S. S.; Ostrovskaya, L. K.; Nazarova, N. Yu.; Karpenko, L. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 7 p. 1438 - 1444
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 7 p. 1580 - 1587
