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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
92964-54-0
合成路线
（共 9 条）
27331-33-5
1-(4-甲氧基苯基)萘
→
反应条件
92964-54-0
反应条件
boron tribromide in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Basaric, Nikola; Doslic, Nacrossed D Signa; Ivkovic, Jakov; Wang, Yu-Hsuan; Veljkovic, Jelena; Mlinaric-Majerski, Kata; Wan, Peter
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1811 - 1823
106-41-2
4-溴苯酚
+
7029-32-5
→
反应条件
92964-54-0
反应条件
[(P{(NC5H10)(C6H11)2})2Pd(Cl)2] in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 2 h; In air;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Chemistry - A European Journal, 2010 , vol. 16, # 36 p. 11072 - 11081
106-41-2
4-溴苯酚
→
反应条件
92964-54-0
反应条件
sodium hydroxide; palladium dichloride in water T=75°C; 3 h;
参考文献
Bumagin, Nikolay A.; Tsarev, Dmitriy A.
Tetrahedron Letters, 1998 , vol. 39, # 44 p. 8155 - 8158
90-11-9
1-溴代萘
+
71597-85-8
4-羟基苯硼酸
→
反应条件
92964-54-0
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Zhao, Yu-Long; Li, You; Li, Shui-Ming; Zhou, Yi-Guo; Sun, Feng-Yi; Gao, Lian-Xun; Han, Fu-She
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1543 - 1550
605-02-7
1-苯基萘
→
反应条件
92964-54-0
反应条件
(ethylenedinitrilo)tetraacetic acid disodium salt; L-proline; DL-threo-1,4-dimercapto-2,3-butanediol in dimethyl sulfoxide; glycerol T=28°C; pH=7.2; 24 h; Microbiological reactionsodium phosphate buffer;
参考文献
Otomatsu, Toshihiko; Bai, Liming; Fujita, Naoya; Shindo, Kazutoshi; Shimizu, Keiko; Misawa, Norihiko
Journal of Molecular Catalysis B: Enzymatic, 2010 , vol. 66, # 1-2 p. 234 - 240
5720-07-0
4-甲氧基苯硼酸
→
反应条件
92964-54-0
反应条件
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / methanol; toluene / 24 h / |Reflux 2: boron tribromide / dichloromethane / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Basaric, Nikola; Doslic, Nacrossed D Signa; Ivkovic, Jakov; Wang, Yu-Hsuan; Veljkovic, Jelena; Mlinaric-Majerski, Kata; Wan, Peter
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1811 - 1823
90-11-9
1-溴代萘
→
反应条件
92964-54-0
反应条件
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / methanol; toluene / 24 h / |Reflux 2: boron tribromide / dichloromethane / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Basaric, Nikola; Doslic, Nacrossed D Signa; Ivkovic, Jakov; Wang, Yu-Hsuan; Veljkovic, Jelena; Mlinaric-Majerski, Kata; Wan, Peter
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1811 - 1823
106-41-2
4-溴苯酚
+
13922-41-3
1-萘硼酸
→
反应条件
92964-54-0
反应条件
C36H44Cl2O2P2Pd2 T=30°C; Suzuki-Miyaura coupling; 6 h; Basic aq. solution;
参考文献
Marziale, Alexander N.; Jantke, Dominik; Faul, Stefan H.; Reiner, Thomas; Herdtweck, Eberhardt; Eppinger, Joerg
Green Chemistry, 2011 , vol. 13, # 1 p. 169 - 177
91-20-3
萘
→
反应条件
92964-54-0
反应条件
(i) AcOH, (ii) Py*HCl; Multistep reaction;
参考文献
Al'perovich,M.A.; Bogolyubskaya,L.T.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, p. 645 - 650,647 - 651
