2,4,6-三乙烯基环硼氧烷合成路线 （共 7 条）
反应条件
in tetrahydrofuran T=-78°C; 2 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 16 p. 2636 - 2644
参考文献
Journal of the American Chemical Society, , vol. 82, p. 4228 - 4233
Journal of Organic Chemistry, , vol. 27, p. 3712
反应条件
(10H)-phenothiazine in water
参考文献
Journal of Organic Chemistry, , vol. 27, p. 3712
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethylene glycol dimethyl ether; water 20 h; Heating;
参考文献
Martinez-Estibalez, Unai; Sotomayor, Nuria; Lete, Esther
Tetrahedron Letters, 2007 , vol. 48, # 16 p. 2919 - 2922
反应条件
sodium hydroxide; palladium diacetate; triphenylphosphine in tetrahydrofuran; water
T=70°C; Suzuki Coupling; 17 h;
参考文献
UNIVERSITY OF DURHAM
Patent: WO2007/93772 A1, 2007 ;
Location in patent: Page/Page column 11; 14-15 ;
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; toluene
T=100°C; Inert atmosphere;
参考文献
VITAE PHARMACEUTICALS, INC.; CLAREMON, David, A.; LEFTHERIS, Katerina; SINGH, Suresh, B.; TICE, Colin, M.; YE, Yuanjie; ZHUANG, Linghang
Patent: WO2010/141424 A1, 2010 ;
Location in patent: Page/Page column 54-55 ;
WO 2010/141424 A1
反应条件
water; potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether
T=90°C; 3 h;
参考文献
GLAXO GROUP LIMITED
Patent: WO2006/14580 A1, 2006 ;
Location in patent: Page/Page column 34 ;
