1: With titanium(IV) isopropylate in diethyl ether T=-78°C; P=2068.65 Torr; 0.5 h; 2: With isopropylmagnesium chloride in diethyl ether T=-78°C; 0.5 h; Further stages.;
参考文献
European Journal of Organic Chemistry, , # 24 p. 4721 - 4727
1: With iodine; borane-pyridine complex in dichloromethane T=20°C; 2 h; 2: With sodium hydroxide; dihydrogen peroxide in methanol; dichloromethane T=0 - 20°C; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 127, # 16 p. 5766 - 5767
titanium tetrachloride in dichloromethane T=-78 - -30°C; further aldehydes and tetraalkylleads; reaction with mixed tetraalkylleads; other conditions; Product distribution;
