1-苯基-1,3-丁二酮合成路线 (共 471 条)
反应条件
samarium (III) iodide in acetonitrile T=-5°C; 3 h;
参考文献
Hao, Wenying; Zhang, Yongmin; Ying, Taokai; Lu, Pin
Synthetic Communications, 1996 , vol. 26, # 12 p. 2421 - 2427
反应条件
(Ph3P)2Pd(Ph)(I) in benzene T=100°C; P=15200 Torr; 18 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 27, # 39 p. 4745 - 4748
反应条件
samarium diiodide in acetonitrile 1 h; Ambient temperature;
参考文献
Ying, Taokai; Bao, Weiliang; Zhang, Yongmin; Xu, Weinming
Tetrahedron Letters, 1996 , vol. 37, # 22 p. 3885 - 3886
参考文献
DE40747 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 1, p. 217
Chemische Berichte, , vol. 20, p. 655
Justus Liebigs Annalen der Chemie, , vol. 291, p. 52
反应条件
acetic acid; zinc in 1,4-dioxane 12 h; Ambient temperature;
参考文献
Katayama, Sadamu; Fukuda, Kinue; Watanabe, Toshio; Yamauchi, Masashige
Synthesis, 1988 , # 3 p. 178 - 183
反应条件
sulfuric acid in acetone 1 h; Ambient temperature;
参考文献
Majetich; Zhang; Dreyer
Tetrahedron Letters, 1993 , vol. 34, # 3 p. 449 - 452
反应条件
Me-IBX in acetone T=20°C; 12 h;
参考文献
Moorthy, Jarugu Narasimha; Singhal, Nidhi; Senapati, Kalyan
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 80 - 84
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=80°C; 60 h;
参考文献
Suzuki, M.; Watanabe, A.; Noyori, R.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 230 - 236
反应条件
sodium hydride in 1,4-dioxane; N,N-dimethyl-formamide 1.) r.t., 0.5 h, 2.) 0.5 h;
参考文献
Gomez, Virginia; Perez-Medrano, Arturo; Muchowski, Joseph M.
Journal of Organic Chemistry, 1994 , vol. 59, # 5 p. 1219 - 1221
反应条件
samarium diiodide in tetrahydrofuran T=20°C; Reformatsky type reaction; 1 h;
参考文献
Baek, Heung Soo; Yoo, Byung Woo; Keum, Sam Rok; Yoon, Cheol Min; Kim, Sung Hoon; Kim, Joong Hyup
Synthetic Communications, 2000 , vol. 30, # 1 p. 31 - 38