1-苯基-1,3-丁二酮合成路线 (共 471 条)
反应条件
AlCl3, aluminium chloride; Oxonereg; in water T=20°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 14 p. 7268 - 7273
反应条件
anhydrous iron chloride; tert.-butylnitrite T=30°C; 12 h; Under airNeat (no solvent);
参考文献
Journal of Organic Chemistry, , vol. 76, # 14 p. 5732 - 5737
反应条件
triethylamine in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Kitamura, Mitsuru; Kato, So; Yano, Masakazu; Tashiro, Norifumi; Shiratake, Yuichiro; Sando, Mitsuyoshi; Okauchi, Tatsuo
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 25 p. 4397 - 4406
反应条件
oxygen; CaI2 10 h; Irradiation;
参考文献
Kanai, Naohiko; Nakayama, Hiroki; Tada, Norihiro; Itoh, Akichika
Organic Letters, 2010 , vol. 12, # 9 p. 1948 - 1951
反应条件
1: carbon disulfide; 1-phenylbutane-1,3-dione With tetrabutylammomium bromide; potassium carbonate in water T=20°C; 1 h; 2: Me-X, X = Hal in water T=20°C; 8.25 h; Further stages.;
参考文献
Fu, Zhenqian; Wang, Mang; Ma, Yuhui; Liu, Qun; Liu, Jun
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7625 - 7630
反应条件
(i) aq. NaOH, <nBu4N>HSO4, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Liang, Deqiang; Wang, Mang; Bekturhun, Bahargul; Xiong, Binbin; Liu, Qun
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1593 - 1599
反应条件
(i) KNH2, liq. NH3, Et2O, (ii) /BRN= 386547/; Multistep reaction;
参考文献
Sugiyama,N. et al.
Bulletin of the Chemical Society of Japan, 1969 , vol. 42, p. 1357 - 1359
反应条件
1: hydrazine hydrate View Scheme
参考文献
v. Auwers; Stuhlmann
Chemische Berichte, 1926 , vol. 59, p. 1054
参考文献
Singh,R.V.; Tandon,J.P.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical, 1978 , vol. 16A, p. 1062 - 1065
参考文献
Escale,R. et al.
Bulletin de la Societe Chimique de France, 1974 , p. 725 - 733