1-苯基-1,3-丁二酮合成路线 (共 471 条)
反应条件
in xylene 14 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 22, # 5 p. 499 - 501
反应条件
copper(l) iodide; K3PO4*3H2O in dimethyl sulfoxide T=90°C; 20 h; Inert atmosphere;
参考文献
He, Chuan; Guo, Sheng; Huang, Li; Lei, Aiwen
Journal of the American Chemical Society, 2010 , vol. 132, # 24 p. 8273 - 8275
反应条件
potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate in N,N-dimethyl-formamide T=20°C;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 18 p. 2363 - 2368
反应条件
water; toluene-4-sulfonic acid in acetonitrile T=80°C; 16 h; Sealed tube;
参考文献
Mayo, Muhammad Shareef; Yu, Xiaoqiang; Zhou, Xiaoyu; Feng, Xiujuan; Yamamoto, Yoshinori; Bao, Ming
Organic Letters, 2014 , vol. 16, # 3 p. 764 - 767
反应条件
dihydrogen peroxide in water T=25°C; 8 h; Green chemistry;
参考文献
Sun, Xi; Wang, Min; Li, Pinhua; Zhang, Xiuli; Wang, Lei
Green Chemistry, 2013 , vol. 15, # 12 p. 3289 - 3294
反应条件
diisopropylamine in tetrahydrofuran
参考文献
SmithKline Beecham Corporation
Patent: US6498174 B1, 2002 ;
反应条件
potassium fluoride; palladium diacetate; chlorobenzene in tetrahydrofuran; water T=20°C; 1 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 4 p. 584 - 587
反应条件
potassium fluoride; palladium diacetate; chlorobenzene in tetrahydrofuran; water T=20°C; 1 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 4 p. 584 - 587
反应条件
1: 34 percent / sodium hydride / tetrahydrofuran / Ambient temperature 2: 79 percent / NaBH4, NiCl2*6H2O / methanol / ice-cooling View Scheme
参考文献
Wang, Feng; Chiba, Kazuhiro; Tada, Masahiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 15 p. 1897 - 1900
反应条件
sodium tetrahydroborate; sodium hydride; nickel dichloride 1) THF, room temperature, 2) MeOH, ice cooling; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Wang, Feng; Chiba, Kazuhiro; Tada, Masahiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 15 p. 1897 - 1900