1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
anhydrous iron chloride; tert.-butylnitrite
T=30°C; 12 h; Under airNeat (no solvent);
参考文献
Huang, Lehao; Cheng, Kai; Yao, Bangben; Xie, Yongju; Zhang, Yuhong
Journal of Organic Chemistry, 2011 , vol. 76, # 14 p. 5732 - 5737
反应条件
in tetrahydrofuran
6 h; Reflux;
参考文献
Eakta; Aggarwal, Ranjana; Sumran, Garima
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 2 p. 273 - 281
反应条件
tetraphosphorus decasulfide; potassium iodide
1.) xylene, 120 degC, 2h 2.) H2O; Yield given. Multistep reaction;
参考文献
Sauve, Jean-Pierre; Lozac'H, Noel
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 11-12 p. 577 - 581
反应条件
sodium acetate in ethanol
Condensation; 3 h; Heating;
参考文献
Genin, Michael J.; Biles, Carolyn; Keiser, Barb J.; Poppe, Susan M.; Swaney, Steven M.; Tarpley, W. Gary; Yagi, Yoshihiko; Romero, Donna L.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 5 p. 1034 - 1040
反应条件
aluminum oxide
T=110°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Norris, Timothy; Colon-Cruz, Roberto; Ripin, David H. B.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 10 p. 1844 - 1849
反应条件
1: 92 percent / BF3*Et2O / 6 h / 20 °C
2: 83 percent / acetonitrile / 2 h / 20 °C
View Scheme
参考文献
Stefane, Bogdan; Polanc, Slovenko
New Journal of Chemistry, 2002 , vol. 26, # 1 p. 28 - 32
反应条件
toluene-4-sulfonic acid in ethanol
16 h; Heating;
参考文献
Haddad, Nizar; Baron, James
Tetrahedron Letters, 2002 , vol. 43, # 12 p. 2171 - 2173
反应条件
hydrogenchloride in N,N-dimethyl acetamide
T=20°C; 24 h; Product distribution; Further Variations:SolventsTemperatures;
参考文献
Gosselin, Francis; O'Shea, Paul D.; Webster, Robert A.; Reamer, Robert A.; Tillyer, Richard D.; Grabowski, Edward J. J.
Synlett, 2006 , # 19 p. 3267 - 3270
反应条件
potassium hydrogensulfate; (NH4)2CO3; silica gel
T=20°C; 0.166667 h;
参考文献
Xu, Shi-Liang; Li, Cheng-Ping; Li, Jing-Hua
Synlett, 2009 , # 5 p. 818 - 822
反应条件
(NH4)2CO3 in ethanol; water
Ambient temperature;
参考文献
Lhotak, Pavel; Kurfuerst, Antonin
Collection of Czechoslovak Chemical Communications, 1992 , vol. 57, # 9 p. 1937 - 1946
