1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
1: 69 percent / TsOH / benzene / Heating
2: 36 percent / Et3N, P(2-CH3C6H4)3 / Pd(OAc)2 / dimethylformamide / 120 °C
View Scheme
参考文献
Sakamoto, Takao; Nagano, Tatsuo; Kondo, Yoshinori; Yamanaka, Hiroshi
Synthesis, 1990 , # 3 p. 215 - 218
反应条件
1: potassium carbonate / dimethyl sulfoxide / 80 - 90 °C
2: iron; acetic acid / 1 h / Reflux
View Scheme
参考文献
Janreddy, Donala; Kavala, Veerababurao; Bosco, J. W. John; Kuo, Chun-Wei; Yao, Ching-Fa
European Journal of Organic Chemistry, 2011 , # 12 p. 2360 - 2365
反应条件
sodium ethanolate in ethanol
Ambient temperature;
参考文献
Hayashi; Furukawa; Yamamoto; Niigata
Chemical and pharmaceutical bulletin, 1967 , vol. 15, # 8 p. 1188 - 1192
反应条件
in ethanol
2 h; Heating;
参考文献
Nishida, Yuzo; Kida, Sigeo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1986 , p. 2633 - 2640
反应条件
diethyl ether; potassium carbonate
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1896 , vol. 291, p. 100
反应条件
potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate in N,N-dimethyl-formamide
T=20°C;
参考文献
Singh, Harjit; Singh, Palwinder; Chimni, Swapandeep Singh; Kumar, Subodh
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 18 p. 2363 - 2368
参考文献
Cirigottis,K.A. et al.
Australian Journal of Chemistry, 1974 , vol. 27, p. 2209 - 2228
反应条件
sodium hydride in dimethyl sulfoxide
参考文献
Gree, Rene; Park, Hokoon; Paquette, Leo A.
Journal of the American Chemical Society, 1980 , vol. 102, # 13 p. 4397 - 4403
反应条件
bismuth trifluoromethanesulphonate in nitromethane
T=100°C; 8.5 h;
参考文献
Rueping, Magnus; Nachtsheim, Boris J.; Kuenkel, Alexander
Organic Letters, 2007 , vol. 9, # 5 p. 825 - 828
反应条件
sodium in acetonitrile
T=90°C; 12 h;
参考文献
Yoshihara, Nobutoshi; Kitagawa, Teruhiro; Ihara, Ikuko; Hasegawa, Sadao; Hasegawa, Tadashi
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 4 p. 1185 - 1187
