1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
sodium in acetonitrile
T=90°C; 12 h;
参考文献
Yoshihara, Nobutoshi; Kitagawa, Teruhiro; Ihara, Ikuko; Hasegawa, Sadao; Hasegawa, Tadashi
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 4 p. 1185 - 1187
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tert-butyl alcohol
7 h; Heating;
参考文献
Marquet, Jorge; Moreno-Manas, Marcial; Pacheco, Pedro; Prat, Maria; Katritzky, Alan R.; Brycki, Bogumil
Tetrahedron, 1990 , vol. 46, # 15 p. 5333 - 5346
反应条件
1: piperidine, B2O3 / benzene
2: HCO2H, Et3N / 145 - 150 °C
View Scheme
参考文献
Sekiya,M.; Suzuki,K.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 1530 - 1534
反应条件
caesium carbonate in acetonitrile
T=100°C;
参考文献
Liu, Lei; Hu, Jie; Wang, Xiang-Chuan; Zhong, Mei-Jin; Liu, Xue-Yuan; Yang, Shang-Dong; Liang, Yong-Min
Tetrahedron, 2012 , vol. 68, # 27-28 p. 5391 - 5395
反应条件
copper(l) iodide; caesium carbonate in dimethyl sulfoxide
T=100°C; 0.5 h; Inert atmosphere;
参考文献
Kavala, Veerababurao; Wang, Cheng-Chuan; Barange, Deepak Kumar; Kuo, Chun-Wei; Lei, Po-Min; Yao, Ching-Fa
Journal of Organic Chemistry, 2012 , vol. 77, # 11 p. 5022 - 5029
反应条件
1: bis(acetylacetonate)nickel(II) / 24 h / 100 °C
2: methanol; sodium / 1 h / Reflux
View Scheme
参考文献
Josefik, Frantisek; Svobodova, Marketa; Bertolasi, Valerio; Simunek, Petr; MacHacek, Vladimir; Almonasy, Numan; Cernoskova, Eva
Journal of Organometallic Chemistry, 2012 , vol. 699, p. 75 - 81
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=68°C; 2 h;
参考文献
Bellur, Esen; Langer, Peter
Tetrahedron, 2006 , vol. 62, # 23 p. 5426 - 5434
反应条件
antimony(V) pentachloride in nitromethane
24 h;
参考文献
Shibaeva, N. V.; Borodaev, S. V.; Luk'yanov, S. M.; Pyshchev, A. I.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2376 - 2377
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2630 - 2631
反应条件
aluminum oxide
T=110°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Norris, Timothy; Colon-Cruz, Roberto; Ripin, David H. B.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 10 p. 1844 - 1849
反应条件
toluene-4-sulfonic acid in ethanol
16 h; Heating;
参考文献
Haddad, Nizar; Baron, James
Tetrahedron Letters, 2002 , vol. 43, # 12 p. 2171 - 2173
