1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
hydrogenchloride in N,N-dimethyl acetamide
T=20°C; 24 h; Product distribution; Further Variations:SolventsTemperatures;
参考文献
Gosselin, Francis; O'Shea, Paul D.; Webster, Robert A.; Reamer, Robert A.; Tillyer, Richard D.; Grabowski, Edward J. J.
Synlett, 2006 , # 19 p. 3267 - 3270
反应条件
in dichloromethane; acetic acid; ethyl acetate
参考文献
E. I. Du Pont de Nemours and Company
Patent: US5127936 A1, 1992 ;
参考文献
Zelenin, Kirill N.; Alekseyev, Valery V.; Tygysheva, Alja R.; Yakimovitch, Stanislav I.
Tetrahedron, 1995 , vol. 51, # 41 p. 11251 - 11256
Title/Abstract View citing articles Show Details
Zelenin; Tugusheva; Yakimovich; Alekseev; Zerova
Chemistry of Heterocyclic Compounds, 2002 , vol. 38, # 6 p. 668 - 676
反应条件
hydrogenchloride in ethanol
5 h; Heating;
参考文献
Kashima, Choji; Katoh, Akira
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 913 - 915
参考文献
Zylewska, Alicja; Tejchman, Waldemar; Korohoda, Maria J.; Zylewski, Marek
Heterocycles, 2003 , vol. 60, # 12 p. 2749 - 2760
反应条件
hydrogenchloride in ethanol
5 h; Heating;
参考文献
Kashima, Choji; Katoh, Akira
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 913 - 915
反应条件
1: 82 percent / hydrochloric acid / ethanol / 5 h / Heating
2: 85 percent / sodium methoxide, methyl iodide / methanol / 3 h / Ambient temperature
View Scheme
参考文献
Kashima, Choji; Katoh, Akira
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 913 - 915
反应条件
1: 1-phenylbutane-1,3-dione With tetrabutylammomium bromide; potassium carbonate in water
T=20°C;
2: carbon disulfide; 2-bromo-1-ethanol in water
T=20°C;
参考文献
Li, Yan; Zhang, Qian; Cheng, Xin; Liu, Qun; Xu, Xiaohong
Synthesis, 2009 , # 5 p. 824 - 828
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; Condensation; cyclization; 5 h;
参考文献
Shu-Jia; Qun; Yao-Zu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 2 p. 147 - 150
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Pratap, Ram; Gupta, R. C.; Srimal, R. C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 8 p. 695 - 698
