1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=0 - 5°C; Yield given;
参考文献
Barros, M. T.; Geraldes, C. F. G. C.; Maycock, C. D.; Silva, M. I.
Tetrahedron, 1988 , vol. 44, # 8 p. 2283 - 2288
反应条件
in butan-1-ol
17 h; Heating;
参考文献
Wendelin, Winfried; Schermanz; Karl; Schweiger, Klaus; Fuchsgruber, Alfred
Monatshefte fuer Chemie, 1983 , vol. 114, p. 1371 - 1380
反应条件
zinc(II) chloride in n-heptane; toluene
33 h; Heating;
参考文献
Ahmed, M. G.; Ahmed, S. A.; Bahar, M. H.; Khondaker, M. A.; Islam, M. A.; Anam, A. K. M. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 470 - 471
参考文献
Ma, Zhen; Maharramov, Abel M.; Aliyev, Ismayil A.; Aliyeva, Irada N.; Kopylovich, Maximilian N.; Amanullayeva, Gunel I.; Mahmudov, Kamran T.; Pombeiro, Armando J.L.
Journal of Molecular Structure, 2012 , vol. 1019, p. 16 - 20
反应条件
1.1: N2H4*H2O / toluene
2.1: NaH / tetrahydrofuran
2.2: tetrahydrofuran / 48 h / Heating
View Scheme
参考文献
Montoya, Vanessa; Pons, Josefina; Branchadell, Vicenc; Ros, Josep
Tetrahedron, 2005 , vol. 61, # 52 p. 12377 - 12385
反应条件
trimeric thionitrosyl chloride; 4 A molecular sieve in tetrachloromethane
12 h; Heating;
参考文献
Duan, Xiao-Guang; Duan, Xiao-Lan; Rees, Charles W.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 19 p. 2831 - 2836
反应条件
Cu(NO3)2*3H2O
T=20°C; 1.33333 h; Neat (no solvent); regioselective reaction;
参考文献
Li, Geng-Chen
Monatshefte fur Chemie, 2008 , vol. 139, # 7 p. 789 - 792
反应条件
formic acid in methanol
48 h; Heating / reflux;
参考文献
SHANGHAI INSTITUTE OF ORGANIC CHEMISTRY, CHINESE ACADEMY OF SCIENCES
Patent: EP2039677 A1, 2009 ;
Location in patent: Page/Page column 9-10 ;
反应条件
0.0833333 h; Microwave irradiation;
参考文献
Goswami, Shyamaprosad; Hazra, Anita; Jana, Subrata
Bulletin of the Chemical Society of Japan, 2009 , vol. 82, # 9 p. 1175 - 1181
反应条件
sodium methylate
1) ethanol, 2) 18 h, reflux; Yield given. Multistep reaction;
参考文献
Wendelin, Winfried; Schermanz; Karl; Schweiger, Klaus; Fuchsgruber, Alfred
Monatshefte fuer Chemie, 1983 , vol. 114, p. 1371 - 1380
