1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
in ethanol
1 h; Heating;
参考文献
Feid-Allah; Soliman
Pharmazie, 1981 , vol. 36, # 7 p. 471 - 473
反应条件
1: 80 percent / ethanol / 1 h / steam bath
2: 32 percent / PPA / 0.42 h / steam bath
View Scheme
参考文献
Amer; Zimmer
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 5 p. 1231 - 1238
反应条件
1: conc. HCl / ethanol / Heating
2: 56 percent / Lawesson's reagent / m-xylene / 1.5 h / Heating
View Scheme
参考文献
Zylewska, Alicja; Tejchman, Waldemar; Korohoda, Maria J.; Zylewski, Marek
Heterocycles, 2003 , vol. 60, # 12 p. 2749 - 2760
反应条件
toluene-4-sulfonic acid in benzene
15 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Nishio, Takehiko; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 934 - 938
参考文献
Yakimovich, S. I.; Nikolaev, V. N.; Kutsenko, E. Yu.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2037 - 2043
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 11 p. 2333 - 2339
参考文献
Yakimovich, S. I.; Nikolaev, V. N.; Kutsenko, E. Yu.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2037 - 2043
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 11 p. 2333 - 2339
反应条件
1: copper(II) oxide; iodine / dimethyl sulfoxide / 12 h / 70 °C
2: hydrazine hydrate / tert-butyl alcohol / |Reflux
View Scheme
参考文献
Gao, Qinghe; Zhu, Yanping; Lian, Mi; Liu, Meicai; Yuan, Jingjing; Wu, Anxin; Yin, Guodong
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9865 - 9870,6
反应条件
N-bromosuccinmide; potassium tert-butylate in ethyl acetate
T=60°C; 6 h; Green chemistry;
参考文献
Chen, Wen-Lin; Li, Ji-Hui; Meng, Xu; Tang, Dong; Guo, Shuai-Bo; Chen, Bao-Hua
Tetrahedron Letters, 2013 , vol. 54, # 4 p. 295 - 299
反应条件
in dimethyl sulfoxide
1.5 h; Heating;
参考文献
Gupta, Radha Raman; Kumar, Rakesh
Heterocycles, 1984 , vol. 22, # 1 p. 87 - 91
反应条件
in ethanol; acetic acid
0.5 h; Heating;
参考文献
Outurquin, Francis; Paulmier, Claude
Bulletin de la Societe Chimique de France, 1983 , vol. 2, # 5-6 p. 159 - 163
