1-苯基-1,3-丁二酮合成路线 (共 471 条)
反应条件
1.1: tetrahydrofuran / 0.5 h / 25 °C 1.2: 97 percent / tetrahydrofuran / 0.5 h / 25 °C 2.1: 83 percent / FeCl3 / tetrahydrofuran / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 122, # 48 p. 12047 - 12048
反应条件
4-methylpyridine 1-oxide; (IPr)AuCl; bis-(trifluoromethylsulphonyl)amine; AgNTf2 in dichloromethane T=20°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 77, # 17 p. 7761 - 7767
反应条件
boron trifluoride in nitromethane T=-35°C; 1 h;
参考文献
Kopka, Ihor; Rathke, Michael W.
Journal of Organic Chemistry, 1981 , vol. 46, # 19 p. 3771 - 3773
反应条件
titanium(IV) bistriflate in dichloromethane 5 h; Ambient temperature;
参考文献
Tanabe, Yoo; Mukaiyama, Teruaki
Chemistry Letters, 1985 , p. 673 - 676
反应条件
1: Et3N / diethyl ether / 0 °C 2: H2 / Ni / methanol; H2O / 760 Torr / Ambient temperature 3: aqeous acid View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 20 p. 2079 - 2082
反应条件
tetrabutyl ammonium fluoride; water in tetrahydrofuran T=60°C; 4 h;
参考文献
Green Chemistry, , vol. 13, # 11 p. 3218 - 3223
反应条件
acetic acid; lithium hexamethyldisilazane in toluene T=0°C; 0.0166667 h; Inert atmosphere;
参考文献
Medicinal Chemistry letters, , vol. 3, # 8 p. 678 - 682,5
ACS Medicinal Chemistry Letters, , vol. 3, # 8 p. 678 - 682
反应条件
triethylamine in dichloromethane
参考文献
Journal of Organic Chemistry, , vol. 51, # 10 p. 1692 - 1700
反应条件
1: H2 / Ni / methanol; H2O / 760 Torr / Ambient temperature 2: aqeous acid View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 20 p. 2079 - 2082
反应条件
tetrakis(triphenylphosphine) palladium(0); methylene bis(iodozinc) in tetrahydrofuran T=25°C; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 5 p. 1389 - 1393