1-苯基-1,3-丁二酮合成路线 (共 471 条)
反应条件
in methanol
T=20°C; Cyclization; Condensation; 6 h;
参考文献
Sawusch, Stefan; Schilde, Uwe
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1999 , vol. 54, # 7 p. 881 - 886
反应条件
[bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate in tetrahydrofuran
T=7°C;
参考文献
Wang, Xianpei; Ma, Lijuan; Yu, Wei
Synthesis, 2011 , # 15 p. 2445 - 2453
反应条件
[bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate in tetrahydrofuran
T=7°C;
参考文献
Wang, Xianpei; Ma, Lijuan; Yu, Wei
Synthesis, 2011 , # 15 p. 2445 - 2453
反应条件
hydrogenchloride in ethanol
4 h; Heating;
参考文献
George, Sumod; Nangia, Ashwini; Bagieu-Beucher, Muriel; Masse, Rene; Nicoud, Jean-Francois
New Journal of Chemistry, 2003 , vol. 27, # 3 p. 568 - 576
反应条件
1: piperidine; magnesium sulfate; acetic acid / toluene / 6 h / 60 °C
2: gold(III) chloride; dihydrogen peroxide / dichloromethane / 12 h / 20 °C
View Scheme
参考文献
Wang, Tao; Zhang, Junliang
Dalton Transactions, 2010 , vol. 39, # 18 p. 4270 - 4273
反应条件
1: selenium(IV) oxide / ethanol; diethyl ether / 5 h / |Reflux
2: ethanol / 3 h / |Reflux
View Scheme
参考文献
Gashaw, Tsegaye; Reda, Gebremedihin; Ayalew, Hailemichael; Babu, Neelaiah; Upadhyay, Rajkumar
Oriental Journal of Chemistry, 2013 , vol. 29, # 3 p. 957 - 962
反应条件
1: selenium(IV) oxide / ethanol; diethyl ether / 5 h / |Reflux
2: ethanol / 3 h / |Reflux
View Scheme
参考文献
Gashaw, Tsegaye; Reda, Gebremedihin; Ayalew, Hailemichael; Babu, Neelaiah; Upadhyay, Rajkumar
Oriental Journal of Chemistry, 2013 , vol. 29, # 3 p. 957 - 962
反应条件
1: selenium(IV) oxide / ethanol; diethyl ether / 5 h / |Reflux
2: ethanol / 3 h / |Reflux
View Scheme
参考文献
Gashaw, Tsegaye; Reda, Gebremedihin; Ayalew, Hailemichael; Babu, Neelaiah; Upadhyay, Rajkumar
Oriental Journal of Chemistry, 2013 , vol. 29, # 3 p. 957 - 962
反应条件
1: selenium(IV) oxide / ethanol; diethyl ether / 5 h / |Reflux
2: ethanol / 3 h / |Reflux
View Scheme
参考文献
Gashaw, Tsegaye; Reda, Gebremedihin; Ayalew, Hailemichael; Babu, Neelaiah; Upadhyay, Rajkumar
Oriental Journal of Chemistry, 2013 , vol. 29, # 3 p. 957 - 962
反应条件
1: selenium dioxide / ethanol / 4 h / Heating
2: 82 percent / diethyl ether
View Scheme
参考文献
Gashaw, Tsegaye; Reda, Gebremedihin; Ayalew, Hailemichael; Babu, Neelaiah; Upadhyay, Rajkumar
Oriental Journal of Chemistry, 2013 , vol. 29, # 3 p. 957 - 962