1-苯基-1,3-丁二酮合成路线 (共 471 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); methylene bis(iodozinc) in tetrahydrofuran T=25°C; Inert atmosphere; diastereoselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 5 p. 1389 - 1393
反应条件
tetrabutyl ammonium fluoride; water in tetrahydrofuran T=60°C; 4 h;
参考文献
Green Chemistry, , vol. 13, # 11 p. 3218 - 3223
反应条件
antimony trichloride in dichloromethane T=0°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5099 - 5102
反应条件
hydrazine in chloroform-d1 T=20°C;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 10 p. 1630 - 1636
Zhurnal Organicheskoi Khimii, , vol. 30, # 10 p. 1548 - 1553
反应条件
1: With ozone in dichloromethane T=-78°C; 2: With dimethylsulfide in dichloromethane T=-78 - 20°C;
参考文献
Synthesis, , # 8 art. no. Z27609SS, p. 1321 - 1324
反应条件
1: With ozone in dichloromethane T=-78°C; 2: With dimethylsulfide in dichloromethane T=-78 - 20°C;
参考文献
Synthesis, , # 8 art. no. Z27609SS, p. 1321 - 1324
反应条件
methylene bis(iodozinc) in tetrahydrofuran T=25°C; Grob type fragmentation; 2 h; Inert atmosphere;
参考文献
Sada, Mutsumi; Furayama, Taniyuki; Komagawa, Shinsuke; Uchiyama, Masanobu; Matsubara, Seijiro
Chemistry - A European Journal, 2010 , vol. 16, # 34 p. 10474 - 10481
反应条件
aluminium trichloride
参考文献
Journal of the American Chemical Society, , vol. 62, p. 1548
反应条件
phenylhydrazine in chloroform-d1 T=20°C;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 10 p. 1630 - 1636
Zhurnal Organicheskoi Khimii, , vol. 30, # 10 p. 1548 - 1553
反应条件
bismuth(III) chloride; sodium iodide in diethyl ether; dichloromethane 0.666667 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 61, # 11 p. 3885 - 3887