1-苯基-1,3-丁二酮合成路线 (共 471 条)
反应条件
quartz tube T=500°C;
反应条件
rhodium (II) acetate in ethylene glycol dimethyl ether 0.166667 h; Ambient temperature;
参考文献
Pellicciari, Roberto; Fringuelli, Renata; Sisani, Ettore; Curini, Massimo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2566 - 2569
反应条件
1: acetonitrile / 24 h / 60 - 70 °C 2: phosphate buffer pH 6 / ethanol / electrochemical reduction 3: aq. hydrochloric acid / Heating View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 40, # 10 p. 831 - 838
反应条件
1: phosphate buffer pH 6 / ethanol / electrochemical reduction 2: aq. hydrochloric acid / Heating View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 40, # 10 p. 831 - 838
反应条件
water; triethylamine T=60°C; 5 h;
参考文献
Green Chemistry, , vol. 13, # 11 p. 3218 - 3223
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C 1.2: 1 h / -78 °C 2.1: 4-methylpyridine 1-oxide; (IPr)AuCl; AgNTf2; bis-(trifluoromethylsulphonyl)amine / dichloromethane / 24 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 77, # 17 p. 7761 - 7767
反应条件
sodium 2.) benzene, room temp., 6 h; Yield given. Multistep reaction;
参考文献
Nishio, Takehiko; Omote, Yoshimori
Synthesis, 1980 , # 12 p. 1013 - 1015
反应条件
calcium carbonate; mercury dichloride in water; acetonitrile 2 h; Heatingexperiments of dethioacetalization; Product distribution;
参考文献
Stahl, Ingfried; Schramm, Berthold; Manske, Rainer; Gosselck, Juergen
Liebigs Annalen der Chemie, 1982 , # 6 p. 1158 - 1172
反应条件
in chloroform-d1 T=20°C;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 10 p. 1630 - 1636
Zhurnal Organicheskoi Khimii, , vol. 30, # 10 p. 1548 - 1553
参考文献
Justus Liebigs Annalen der Chemie, , vol. 308, p. 325