3,4-环氧-1-丁烯合成路线 (共 241 条)
反应条件
tetraphenyl stibonium iodide in dichloromethane T=45°C; 2.5 h; Yield given. Yields of byproduct given;
参考文献
Fujiwara, Masahiro; Baba, Akio; Matsuda, Haruo
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 1351 - 1357
反应条件
hydrogen in ethanol T=30°C; P=4500.45 Torr; Reagent/catalystSolventTemperature;
参考文献
Applied Catalysis A: General, , vol. 445-446, p. 102 - 106
反应条件
hydrogen; silica gel; palladium T=-0.15°C; P=150.012 Torr; also ethyloxirane; also with duterium; also over Pt-SiO2; var. temp. and time; Product distributionMechanism;
参考文献
Journal of Catalysis, , vol. 175, # 1 p. 40 - 47
反应条件
hydrogen; lt;Rh(NBD)(PPh3)2gt;lt;ClO4gt; T=30°C; P=760 Torr; 8 h; catalytic hydrogenation of the title compound in the presence of various catalysts (cationic rhodium complexes); influence of the type of catalyst's ligand, reaction time and pressure on the activity of catalysts; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 855 - 860
参考文献
Journal of the American Chemical Society, , vol. 102, # 4 p. 1451
反应条件
T=90°C; 1 h; a new decomposition path of reaction; Mechanism;
参考文献
Malievskii, A. D.; Gorbunova, O. I.; Bondarenko, N. A.; Tsvetkov, E. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 1 p. 158 - 161
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 1 p. 169 - 173
参考文献
BASF
Patent: DE1004614 , 1954 ;
反应条件
bis(η3-allyl-μ-chloropalladium(II)); R,R-C52H44N2O2P2 chiral ligand; sodium carbonate in dichloromethane
14 h; Ambient temperature;
参考文献
Trost, Barry M.; O'Boyle, Brendan M.; Torres, Wildeliz; Ameriks, Michael K.
Chemistry - A European Journal, 2011 , vol. 17, # 28 p. 7890 - 7903
反应条件
tetrabutyl-ammonium chloride; lithium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in toluene
T=40°C; Substitution; 40 h; Title compound not separated from byproducts;
参考文献
Harris, Michael C. J.; Jackson, Mark; Lennon, Ian C.; Ramsden, James A.; Samuel, Helen
Tetrahedron Letters, 2000 , vol. 41, # 17 p. 3187 - 3191
反应条件
sodium carbonate; (R,R)-DACH-naphthyl Trost ligand; bis(η3-allyl-μ-chloropalladium(II)) in dichloromethane
Ambient temperature; Yields of byproduct given;
参考文献
Trost, Barry M.; Bunt, Richard C.
Angewandte Chemie, 1996 , vol. 108, # 1 p. 70 - 73