反应条件
1: 1.) butyllithium / 1.) THF, hexane, -78 degC, 2.) 25 degC, 1h
2: 1.) diisobutylaluminium hydride, 2.) bromine / 1.) THF, hexane, 0 degC, 15 min, 25 degC, 4h, 2.) CH2Cl2, THF, hexane, -78 degC, 15 min
3: 93 percent / sodium methoxide / methanol / 4 h / 40 °C
View Scheme
参考文献
Miller,R.B.; McGarvey,G.
Journal of Organic Chemistry, 1978 , vol. 43, p. 4424 - 4431
