ALFA, ALFA-二甲基苄氯合成路线 （共 79 条）
反应条件
.alpha.,.alpha.,.alpha.-trichloroacetamide; triphenylphosphine in dichloromethane T=30°C; 0.25 h;
参考文献
Tetrahedron Letters, , vol. 47, # 38 p. 6821 - 6823
参考文献
Helvetica Chimica Acta, , vol. 40, p. 1639,1650
Journal of the American Chemical Society, , vol. 79, p. 1903,1905
反应条件
1: 67 percent / HCl / 5.5 h / 0 °C 2: 73 percent / butyllithium / tetrahydrofuran; hexane / 1 h / -100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 23 p. 4804 - 4806
参考文献
US5461067 A1, ;
US 5461067 A
反应条件
cation exchange resin KU-2 in H+ form T=150°C; 6 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 21, # 11 p. 1297 - 1298
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 21, # 11 p. 1571 - 1572
反应条件
T=200 - 250°C; Further byproducts given;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 322, # 5 p. 751 - 760
反应条件
1.2: Acidic conditions 2.1: hydrogenchloride / pentane View Scheme
参考文献
International Journal of Chemical Kinetics, , vol. 44, # 8 p. 514 - 523
反应条件
hydrogenchloride; phosphorus pentachloride Multistep reaction;
参考文献
Angewandte Chemie, , vol. 92, # 11 p. 933 - 934
反应条件
2: HCl / Eingiessen des Reaktionsproduktes in Eiswasser View Scheme
参考文献
Chemische Berichte, , vol. 35, p. 2649
Chemische Berichte, , vol. 39, p. 2591
