4,4-二甲氧基-2,5-环己二烯-1-酮合成路线 (共 49 条)
反应条件
pyridine T=125°C; 2 h; Microwave irradiationInert atmosphere;
参考文献
Zhang, Jinzhu; Yin, Zhiwei; Leonard, Patrick; Wu, Jing; Sioson, Kate; Liu, Che; Lapo, Robert; Zheng, Shengping
Angewandte Chemie - International Edition, 2013 , vol. 52, # 6 p. 1753 - 1757
Angew. Chem., 2013 , vol. 125, # 6 p. 1797 - 1801,5
反应条件
[bis(acetoxy)iodo]benzene in methanol
T=20°C; 0.666667 h;
参考文献
Hammill, Jared T.; Contreras-Garcia, Julia; Virshup, Aaron M.; Beratan, David N.; Yang, Weitao; Wipf, Peter
Tetrahedron, 2010 , vol. 66, # 31 p. 5852 - 5862
反应条件
acetic acid in tetrahydrofuran; water
T=70°C; 6 h;
参考文献
Bayer CropScience AG
Patent: US2010/217018 A1, 2010 ;
Location in patent: Page/Page column 3 ;
反应条件
lithium perchlorate; lithium carbonate in methanol; acetonitrile
1.2 V vs. SCE, platinum anode, 2.1 F mol-1;
参考文献
Stewart, Ray F.; Miller, Larry L.
Journal of the American Chemical Society, 1980 , vol. 102, # 15 p. 4999 - 5004
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=0°C; 0.025 h;
参考文献
Stern, Alan; Swenton, John S.
Journal of Organic Chemistry, 1987 , vol. 52, # 13 p. 2763 - 2768
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=0°C; 0.0833333 h;
参考文献
Stern, Alan; Swenton, John S.
Journal of Organic Chemistry, 1987 , vol. 52, # 13 p. 2763 - 2768
反应条件
[bis(acetoxy)iodo]benzene in methanol
Ambient temperature;
参考文献
Pelter, Andrew; Elgendy, Said
Tetrahedron Letters, 1988 , vol. 29, # 6 p. 677 - 680
反应条件
[bis(acetoxy)iodo]benzene in methanol
T=20°C; 0.666667 h;
参考文献
Pelter, Andrew; Elgendy, Said M. A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 16 p. 1891 - 1896
反应条件
potassium chloride in methanol; water
Ambient temperatureelectrolysis;
参考文献
Dhanalekshmi; Balasubramanian; Venkatachalam
Tetrahedron Letters, 1991 , vol. 32, # 51 p. 7591 - 7592
反应条件
potassium chloride in methanol; water
Ambient temperatureelectrolysis;
参考文献
Dhanalekshmi; Balasubramanian; Venkatachalam
Tetrahedron Letters, 1991 , vol. 32, # 51 p. 7591 - 7592