4,4-二甲氧基-2,5-环己二烯-1-酮合成路线 （共 49 条）
反应条件
potassium chloride in methanol; water
Ambient temperatureelectrolysis;
参考文献
Dhanalekshmi; Balasubramanian; Venkatachalam
Tetrahedron Letters, 1991 , vol. 32, # 51 p. 7591 - 7592
反应条件
[bis(acetoxy)iodo]benzene; silica gel; triethylamine
T=20°C; 4 h;
参考文献
Bodipati, Naganjaneyulu; Peddinti, Rama Krishna
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 23 p. 4549 - 4553
反应条件
aluminum oxide in ethyl acetate
参考文献
Coutts, Ian G. C.; Culbert, Nicholas J.; Edwards, Mark; Hadfield, John A.; Musto, Donald R.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1829 - 1836
反应条件
aluminum oxide in ethyl acetate
参考文献
Coutts, Ian G. C.; Culbert, Nicholas J.; Edwards, Mark; Hadfield, John A.; Musto, Donald R.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1829 - 1836
反应条件
in acetonitrile
T=20°C; 19 h;
参考文献
Carreno, M. Carmen; Mudarra, Gerardo Fernandez; Merino, Estibaliz; Ribagorda, Maria
Journal of Organic Chemistry, 2004 , vol. 69, # 10 p. 3413 - 3416
反应条件
[bis(acetoxy)iodo]benzene; silica gel; triethylamine
T=20°C; 5 h;
参考文献
Bodipati, Naganjaneyulu; Peddinti, Rama Krishna
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 23 p. 4549 - 4553
反应条件
2,6-dimethylpyridine; lithium perchlorate in acetonitrile
Electrochemical reaction;
参考文献
Deffieux, Denis; Fabre, Isabelle; Courseille, Christian; Quideau, Stephane
Journal of Organic Chemistry, 2002 , vol. 67, # 13 p. 4458 - 4465
反应条件
2,6-dimethylpyridine; lithium perchlorate in acetonitrile
Electrochemical reaction;
参考文献
Deffieux, Denis; Fabre, Isabelle; Courseille, Christian; Quideau, Stephane
Journal of Organic Chemistry, 2002 , vol. 67, # 13 p. 4458 - 4465
反应条件
sodium cyanide
(electrolysis);
参考文献
Weinberg,N.L. et al.
Journal of the American Chemical Society, 1975 , vol. 97, p. 1499 - 1504
反应条件
1: triethylamine / CH2Cl2 / 1 h / Ambient temperature
2: 100 percent / methanol / Ambient temperature; anodic oxidation, graphite felt anode, platinum cathode, one compartment cell, tetraethylammonium perchlorate
3: 98 percent / neutral alumina column / ethyl acetate
View Scheme
参考文献
Coutts, Ian G. C.; Culbert, Nicholas J.; Edwards, Mark; Hadfield, John A.; Musto, Donald R.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1829 - 1836
