反应条件
1: 60 percent / aq. NaOH / dioxane / 2.5 h / 180 °C 2: LiAlH4 / tetrahydrofuran / 1) reflux, 1 h; 2) rt, 4 h 3: 1.) p-toluenesulfonic acid chloride, pyridine, 2.) LiCl / 1) overnight; 2) 24 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 14 p. 4581 - 4586