in dichloromethane
stirred under ice-cooling for 2.5 h; MCPBA filtered off, organic layer treated with aq. sodium hydrogensulfite, sodium carbonate and NH4Cl, dried (MgSO4), distd.;
参考文献
Takeuchi; Tanaka; Harazono
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 1 p. 91 - 98
sodium hydrogencarbonate in dichloromethane; water
1.5 h; Ambient temperatureother methyl cinnamate derivatives, other temperatures, other reaction times, sodium bicarbonate and water absence; Product distributionMechanism;
参考文献
Moyna, Guillermo; Williams, Howard J.; Scott
Synthetic Communications, 1996 , vol. 26, # 11 p. 2235 - 2239