N-苄基-N-甲基亚硝酰胺合成路线 （共 24 条）
反应条件
sodium tetrahydroborate; titanium tetrachloride in ethylene glycol dimethyl ether 14 h; Ambient temperature;
参考文献
Kano, Shinzo; Tanaka, Yasuyuki; Sugino, Eiichi; Shibuya, Shiroshi; Hibino, Satoshi
Synthesis, 1980 , # 9 p. 741 - 742
反应条件
oxygen in acetonitrile T=25°C; radical reaction; Photolysis; KineticsQuantum yield;
参考文献
Fiz; Usero; Casado
International Journal of Chemical Kinetics, 1993 , vol. 25, # 5 p. 341 - 351
反应条件
TBBDA; water; silica gel; sodium nitrite in dichloromethane
T=20°C; 0.05 h; Reagent/catalyst;
参考文献
Ghorbani-Vaghei, Ramin; Shiri, Lotfi; Ghorbani-Choghamarani, Arash
Letters in Organic Chemistry, 2013 , vol. 10, # 3 p. 204 - 208
反应条件
sodium nitrite in water; acetic acid
T=20°C; Nitrosation;
参考文献
Loeppky, Richard N.; Elomari, Saleh
Journal of Organic Chemistry, 2000 , vol. 65, # 1 p. 96 - 103
反应条件
nitric acid; acetic anhydride
1.) 50 deg C, 30 min, 2.) room temp., 16 h;
参考文献
Boyer; Pillai; Ramakrishnan
Synthesis, 1985 , vol. NO. 6-7, p. 677 - 677
反应条件
hydrogenchloride; nitric acid; acetic anhydride
T=25°C; 16 h;
参考文献
Boyer; Pillai; Ramakrishnan
Synthesis, 1985 , vol. NO. 6-7, p. 677 - 677
反应条件
hydrogenchloride; dinitrogen tetraoxide in acetic anhydride
T=25°C; 14 h;
参考文献
Boyer, Joseph H.; Pillai, T. Perumal
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1661 - 1664
反应条件
1: 68 percent / NaCNBH3; HCl / methanol / 48 h / 20 °C
2: 88 percent / NaNO2 / acetic acid; H2O / 20 °C
View Scheme
参考文献
Loeppky, Richard N.; Elomari, Saleh
Journal of Organic Chemistry, 2000 , vol. 65, # 1 p. 96 - 103
反应条件
1: 78 percent / NaCNBH3; HCl / methanol / 72 h / 20 °C
2: 68 percent / NaCNBH3; HCl / methanol / 48 h / 20 °C
3: 88 percent / NaNO2 / acetic acid; H2O / 20 °C
View Scheme
参考文献
Loeppky, Richard N.; Elomari, Saleh
Journal of Organic Chemistry, 2000 , vol. 65, # 1 p. 96 - 103
反应条件
in tetrahydrofuran
T=25 - 35°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cooper, Curt S.; Peyton, Albert L.; Weinkam, Robert J.
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4116 - 4119
