aluminium trichloride in neat (no solvent) 1.) cooled by tap water, 16 h, 2.) 80 deg C, 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 65, # 1 p. 224 - 225
phosphorus pentachloride in neat (no solvent) 1.) 110-120 deg C, 1 h, 2.) room temp., 2.5 h then 90 deg C, 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 65, # 1 p. 224 - 225
